3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline

Base Information

• Chemical Name: 3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline
• CAS No.: 1799733-46-2
• Molecular Formula: C13H11ClF2N2O
• Molecular Weight: 284.69
• Mol file: 1799733-46-2.mol

Synonyms:3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline

Chemical Property of 3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline

Chemical Property:

• Boiling Point: 347.4±37.0 °C(Predicted)
• PKA: -4.01±0.48(Predicted)
• PSA: 35.01000
• Density: 1.302±0.06 g/cm3(Predicted)
• LogP: 3.95970

Purity/Quality:

99.9% ^*data from raw suppliers

3-Chloro-2-(1,1-difluorobut-3-en-1-yl)-6-methoxyquinoxaline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline

There total 11 articles about 3-chloro-2-(1,1-difluorobut-3-enyl)-6-methoxyquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H13F2N3O → 3-chloro-2-(1,1-difluorobut-3-en-1-yl)-6-methoxyquinoxaline (1799733-46-2)

Guidance literature:

C₁₃H₁₃F₂N₃O; With boron trichloride; In dichloromethane; at 5 ℃; for 0.25h;

With 2-Methyl-2-nitropropane; In dichloromethane; at 5 - 20 ℃; for 14h;

Reference yield:

C13H12F2N2O2 → 3-chloro-2-(1,1-difluorobut-3-en-1-yl)-6-methoxyquinoxaline (1799733-46-2)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; at 30 - 75 ℃;

Reference yield:

3,3-difluoro-2-oxo-5-hexenoic acid + 4-methoxy-1,2-phenylenediamine (102-51-2) → 3-chloro-2-(1,1-difluorobut-3-en-1-yl)-6-methoxyquinoxaline (1799733-46-2)

Guidance literature:

4-methoxy-1,2-phenylenediamine; With triethylamine; In ethanol; at 25 ℃; for 0.25h;

3,3-difluoro-2-oxo-5-hexenoic acid; With acetic acid; In ethanol; at 22 ℃;

With trichlorophosphate; In N,N-dimethyl-formamide; at 30 - 75 ℃; for 0.05h;

upstream raw materials:

ethyl 3,3-difluoro-2-oxo-5-hexenoate

4-methoxy-1,2-phenylenediamine

aniline

2,2-difluoropent-4-enoic acid

Downstream raw materials:

C₃₁H₄₀F₂N₄O₇