3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid

Base Information

Chemical Name:3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid
CAS No.:887242-59-3
Molecular Formula:C16H17NO4
Molecular Weight:287.315
Hs Code.:2924299090
Mol file:887242-59-3.mol

Synonyms:3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid

Suppliers and Price of 3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Boc-3-amino-2-naphthoicAcid
25mg
$ 45.00

Matrix Scientific
Boc-3-amino-2-naphthoic acid
1g
$ 162.00

Matrix Scientific
Boc-3-amino-2-naphthoic acid
5g
$ 585.00

Crysdot
3-((tert-Butoxycarbonyl)amino)-2-naphthoicacid 95+%
10g
$ 452.00

Chemenu
Boc-3-amino-2-naphthoicacid 95%
10g
$ 427.00

Biosynth Carbosynth
Boc-3-amino-2-naphthoic acid
1 g
$ 167.60

Biosynth Carbosynth
Boc-3-amino-2-naphthoic acid
500 mg
$ 65.00

Biosynth Carbosynth
Boc-3-amino-2-naphthoic acid
2 g
$ 268.10

Biosynth Carbosynth
Boc-3-amino-2-naphthoic acid
5 g
$ 429.00

American Custom Chemicals Corporation
3-([(TERT-BUTOXY)CARBONYL]AMINO)NAPHTHALENE-2-CARBOXYLIC ACID 95.00%
5G
$ 1168.42

Total 10 raw suppliers

Chemical Property of 3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid

Chemical Property:

Boiling Point:399.3±25.0 °C(Predicted)
PKA:4.23±0.30(Predicted)
PSA：75.63000
Density:1.276±0.06 g/cm3(Predicted)
LogP:3.95800
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Boc-3-amino-2-naphthoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid

There total 5 articles about 3-((tert-Butoxycarbonyl)aMino)-2-naphthoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: methyl 3-[(tert-butoxycarbonyl)amino]naphthalene-2-carboxylate

: 887242-59-3
3-(tert-butoxycarbonylamino)naphthalene-2-carboxylic acid

Guidance literature:: With methanol; potassium hydroxide; at 20 ℃; for 12h;

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 5959-52-4
2-Amino-3-naphthoic acid

: 887242-59-3
3-(tert-butoxycarbonylamino)naphthalene-2-carboxylic acid

Guidance literature:: With potassium carbonate; In 1,4-dioxane; water; at 0 - 20 ℃; for 10h;
DOI:10.1021/jm300043c

Reference yield:

: 643-79-8
o-phthalic dicarboxaldehyde

: 887242-59-3
3-(tert-butoxycarbonylamino)naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: tributylphosphine / dichloromethane / 0 - 20 °C

1.2: 3 h / 20 °C / Cooling with ice

2.1: potassium hydroxide; methanol / 24 h / 20 °C / Cooling with ice

3.1: diphenyl phosphoryl azide; triethylamine / 27 h / 20 °C / Reflux

4.1: potassium hydroxide; methanol / 12 h / 20 °C

With methanol; tributylphosphine; diphenyl phosphoryl azide; triethylamine; potassium hydroxide; In dichloromethane;