Carbonocyanidothioic amide, methylphenyl- (9CI)

Base Information

• Chemical Name: Carbonocyanidothioic amide, methylphenyl- (9CI)
• CAS No.: 4955-83-3
• Molecular Formula: C9H8N2S
• Molecular Weight: 176.242
• Mol file: 4955-83-3.mol

Synonyms:Carbonocyanidothioic amide, methylphenyl- (9CI)

Chemical Property of Carbonocyanidothioic amide, methylphenyl- (9CI)

Chemical Property:

• PSA: 59.12000
• LogP: 1.97378

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbonocyanidothioic amide, methylphenyl- (9CI)

There total 4 articles about Carbonocyanidothioic amide, methylphenyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl sulfate (77-78-1) + 1-cyanothioformanilide (4955-82-2) → methyl-phenyl-thiooxalamonitrile (4955-83-3,54077-84-8)

Guidance literature:

With sodium hydroxide;

Reference yield:

C14H13NO2S2 (38930-63-1) + potassium cyanide (151-50-8) → methyl-phenyl-thiooxalamonitrile (4955-83-3,54077-84-8)

Guidance literature:

In water; acetone;

DOI:10.1055/s-1972-21878

Reference yield:

phenyl isothiocyanate (103-72-0) → methyl-phenyl-thiooxalamonitrile (4955-83-3,54077-84-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous alcohol

2: NaOH-solution

With sodium hydroxide; ethanol;

upstream raw materials:

dimethyl sulfate

1-cyanothioformanilide

C₁₄H₁₃NO₂S₂

potassium cyanide

Downstream raw materials:

N-methylaniline