1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

Base Information

Chemical Name:1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene
CAS No.:1279691-35-8
Molecular Formula:C₂₃H₂₇ClO₈
Molecular Weight:466.916
Hs Code.:
Mol file:1279691-35-8.mol

Synonyms:1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

Suppliers and Price of 1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 12 raw suppliers

Chemical Property of 1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

There total 3 articles about 1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₆ClO₈^(1-)*Cl^(1-)*Mg⁽²⁺⁾

: 1279691-35-8
(2S,3R,4S,6R)-2-(4-chloro-3-(4-(((S)-tetrahydrofuran-3-yl)oxy)benzyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetraol

Guidance literature:: With citric acid; In water; at -13 - 19 ℃; for 1.41667h; Product distribution / selectivity;

Reference yield:

: 90-80-2,1335-57-5,4253-68-3
D-Glucono-1,5-lactone

: 1279691-35-8
(2S,3R,4S,6R)-2-(4-chloro-3-(4-(((S)-tetrahydrofuran-3-yl)oxy)benzyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-2,3,4,5-tetraol

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / -20 °C / Inert atmosphere; Large scale

1.2: 7 h / 10 °C / Large scale

2.1: lithium chloride; isopropylmagnesium chloride / acetonitrile / 1 h / -20 - -15 °C / Large scale

2.2: 8 h / -10 - 0 °C / Large scale

With pyridine; isopropylmagnesium chloride; lithium chloride; In dichloromethane; acetonitrile;