Dimethyl 2-(4-(methylsulfonyl)-2-nitrophenyl)malonate

Base Information

• Chemical Name: Dimethyl 2-(4-(methylsulfonyl)-2-nitrophenyl)malonate
• CAS No.: 917562-22-2
• Molecular Formula: C12H13NO8S
• Molecular Weight: 331.303
• Hs Code.: 2917399090
• Mol file: 917562-22-2.mol

Synonyms:dimethyl 2-(4-methylsulfonyl-2-nitrophenyl)propanedioate;

Chemical Property of Dimethyl 2-(4-(methylsulfonyl)-2-nitrophenyl)malonate

Chemical Property:

• PSA: 140.94000
• LogP: 2.03190
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

Dimethyl2-(4-(methylsulfonyl)-2-nitrophenyl)malonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dimethyl 2-(4-(methylsulfonyl)-2-nitrophenyl)malonate

There total 1 articles about Dimethyl 2-(4-(methylsulfonyl)-2-nitrophenyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-chloro-4-methanesulfonyl-2-nitrobenzene (97-07-4) → C12H13NO8S (917562-22-2)

Guidance literature:

malonic acid dimethyl ester; With potassium tert-butylate; In tert-butyl alcohol;

1-chloro-4-methanesulfonyl-2-nitrobenzene; In tert-butyl alcohol; at 20 ℃; for 15h; Heating / reflux;

Reference yield: 37.0%

C12H13NO8S (917562-22-2) → C10H11NO6S (1001420-10-5)

Guidance literature:

With water; sodium chloride; In dimethyl sulfoxide; at 120 ℃; for 5h;

upstream raw materials:

1-chloro-4-methanesulfonyl-2-nitrobenzene

Downstream raw materials:

C₁₀H₁₁NO₆S

Refernces