N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine

Base Information

Chemical Name:N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine
CAS No.:227804-35-5
Molecular Formula:C₉H₁₃NO₃
Molecular Weight:183.207
Hs Code.:
DSSTox Substance ID:DTXSID101272344
Mol file:227804-35-5.mol

Synonyms:227804-35-5;N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine;DTXSID101272344;AKOS021002971;N-Hydroxy-3,4-dimethoxybenzenemethanamine;FT-0701769;EN300-1830081

Suppliers and Price of N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:183.08954328
Heavy Atom Count:13
Complexity:143

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CNO)OC

Technology Process of N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine

There total 3 articles about N-[(3,4-dimethoxyphenyl)methyl]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2169-98-4,39627-82-2
3,4-Dimethoxy-benzaldehyde oxime

: 227804-35-5
N-(3,4-dimethoxybenzyl)hydroxylamine

Guidance literature:: With sodium cyanoborohydride;
DOI:10.1055/s-1999-2672

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 227804-35-5
N-(3,4-dimethoxybenzyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium hydroxide / water / 2 h / 0 °C

2: sodium cyanoborohydride; hydrogenchloride / methanol

With hydrogenchloride; hydroxylamine hydrochloride; sodium cyanoborohydride; sodium hydroxide; In methanol; water;
DOI:10.1139/cjc-2012-0199