3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one

Base Information

Chemical Name:3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one
CAS No.:17014-58-3
Molecular Formula:C₁₇H₁₇NO₆
Molecular Weight:331.325
Hs Code.:
Mol file:17014-58-3.mol

Synonyms:3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one

Suppliers and Price of 3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one

Chemical Property:

Boiling Point:480.4±45.0 °C(Predicted)
PKA:11.22±0.40(Predicted)
Density:1.46±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one

There total 6 articles about 3a,11b-Dihydro-5-hydroxy-4,11b-dimethoxy-11-methyl-1,3-dioxolo[4,5-c]acridin-6(11H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14382-74-2
4,11b-dimethoxy-11-methyl-11H,11bH-[1,3]dioxolo[4,5-c]acridine-4,5-dione

: 14382-75-3,17014-58-3
4,11b-dimethoxy-11-methyl-3a,11b-dihydro-4H,11H-[1,3]dioxolo[4,5-c]acridine-5,6-dione; enol tautomer

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol;

Reference yield:

: 14382-74-2
4,11b-dimethoxy-11-methyl-11H,11bH-[1,3]dioxolo[4,5-c]acridine-4,5-dione

: 14382-75-3,17014-58-3
5-hydroxy-4,11b-dimethoxy-11-methyl-(3ar,11bc)-3a,11b-dihydro-11H-[1,3]dioxolo[4,5-c]acridin-6-one

Guidance literature:: With sodium tetrahydroborate; at 0 ℃;
DOI:10.1016/S0040-4039(00)70113-4

Reference yield:

: 568-01-4
4,5-dimethoxy-11-methyl-11H-[1,3]dioxolo[4,5-c]acridin-6-one

: 14382-75-3,17014-58-3
5-hydroxy-4,11b-dimethoxy-11-methyl-(3ar,11bc)-3a,11b-dihydro-11H-[1,3]dioxolo[4,5-c]acridin-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂ / methanol

2: OH^-

3: NaBH₄ / 0 °C

With sodium tetrahydroborate; hydroxide; bromine; In methanol;
DOI:10.1016/S0040-4039(00)70113-4