methyl 4-acetoxy-6-benzyloxy-7-methoxy-naphthalene-2-carboxylate

Base Information

• Chemical Name: methyl 4-acetoxy-6-benzyloxy-7-methoxy-naphthalene-2-carboxylate
• CAS No.: 95626-14-5
• Molecular Formula: C₂₂H₂₀O₆
• Molecular Weight: 380.397

Synonyms:2-Naphthalenecarboxylic acid, 4-(acetyloxy)-7-Methoxy-6-(phenylMethoxy)-, Methyl ester

Chemical Property of methyl 4-acetoxy-6-benzyloxy-7-methoxy-naphthalene-2-carboxylate

Chemical Property:

• Vapor Pressure: 9.43E-12mmHg at 25°C
• Boiling Point: 540.6°C at 760 mmHg
• Flash Point: 236.2°C
• PSA: 71.06000
• Density: 1.235g/cm³
• LogP: 4.13930

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 4-acetoxy-6-benzyloxy-7-methoxy-naphthalene-2-carboxylate

There total 1 articles about methyl 4-acetoxy-6-benzyloxy-7-methoxy-naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) + acetic anhydride (108-24-7) + Dimethyl succinate (106-65-0) → 4-Acetoxy-6-benzyloxy-7-methoxy-naphthoesaeure-(2)-methylester (95626-14-5)

Guidance literature:

Multistep reaction; (i) K, tBuOH, (heating), (ii) /BRN= 385737/, NaOAc;

Reference yield:

4-Acetoxy-6-benzyloxy-7-methoxy-naphthoesaeure-(2)-methylester (95626-14-5) → 6-Benzyloxy-4-hydroxy-7-methoxy-naphthoesaeure-(2) (94305-99-4)

Guidance literature:

With potassium hydroxide; In ethanol; Heating;

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

acetic anhydride

Dimethyl succinate

Downstream raw materials:

6-Benzyloxy-4-hydroxy-7-methoxy-naphthoesaeure-⁽²⁾

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