N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE

Base Information

• Chemical Name: N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE
• CAS No.: 2562-74-5
• Molecular Formula: C17H19N3
• Molecular Weight: 265.358
• Mol file: 2562-74-5.mol

Synonyms:4-(1H-BENZIMIDAZOL-2-YL)-N,N-DIETHYL-BENZENAMINE;N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE;2-[4-(DiethylaMino)phenyl]benziMidazole, 95%;[4-(1H-Benzoimidazol-2-yl)-phenyl]-diethyl-amine

Chemical Property of N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE

Chemical Property:

• PSA: 31.92000
• LogP: 4.07610

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE

There total 1 articles about N-[4-(1H-BENZIMIDAZOL-2-YL)PHENYL]-N,N-DIETHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-Diethylaminobenzaldehyde (120-21-8) + 1,2-diamino-benzene (95-54-5) → 4-(1H-benzo[d]imidazol-2-yl)-N,N-diethylaniline (2562-74-5)

Guidance literature:

With 1,1'-((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(3-propyl-1H-imidazol-3-ium) bromide; In neat (no solvent); for 0.25h; Heating;

DOI:10.1002/jccs.201400372

Reference yield: 85.0%

4-(1H-benzo[d]imidazol-2-yl)-N,N-diethylaniline (2562-74-5) + diphenyl acetylene (501-65-5) → N,N-diethyl-5,6-diphenylbenzo[4,5]imidazo[2,1-a]isoquinolin-3-amine (1447946-56-6)

Guidance literature:

With copper(II) acetate dihydrate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; In water; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2013.05.106

Reference yield: 79.0%

N-(2-chlorethyl)morpholine (3240-94-6) + 4-(1H-benzo[d]imidazol-2-yl)-N,N-diethylaniline (2562-74-5) → 2-(4-diethylaminophenyl)-1-[2-(morpholin-4-yl)ethyl]-1H-benzimidazole

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 170 ℃; for 0.5h; under 7500.75 Torr; Microwave irradiation;

DOI:10.3390/molecules22081374

upstream raw materials:

4-Diethylaminobenzaldehyde

1,2-diamino-benzene

Downstream raw materials:

N,N-diethyl-5,6-diphenylbenzo[4,5]imidazo[2,1-a]isoquinolin-3-amine