1-Phenyl-5,6-dihydro-benzo[f]isoquinoline

Base Information

Chemical Name:1-Phenyl-5,6-dihydro-benzo[f]isoquinoline
CAS No.:131372-97-9
Molecular Formula:C₁₉H₁₅N
Molecular Weight:257.335
Hs Code.:2933990090
DSSTox Substance ID:DTXSID50564268
Wikidata:Q82448916
Mol file:131372-97-9.mol

Synonyms:1-Phenyl-5,6-dihydro-benzo[f]isoquinoline;131372-97-9;1-Phenyl-5,6-dihydrobenzo[f]isoquinoline;DTXSID50564268;J-005984

Suppliers and Price of 1-Phenyl-5,6-dihydro-benzo[f]isoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-PHENYL-5,6-DIHYDRO-BENZO[F]ISOQUINOLINE 95.00%
1G
$ 1049.03

Total 3 raw suppliers

Chemical Property of 1-Phenyl-5,6-dihydro-benzo[f]isoquinoline

Chemical Property:

PSA：12.89000
LogP:4.51420
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:257.120449483
Heavy Atom Count:20
Complexity:320

Purity/Quality:

97% ^*data from raw suppliers

1-PHENYL-5,6-DIHYDRO-BENZO[F]ISOQUINOLINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CN=CC(=C2C3=CC=CC=C31)C4=CC=CC=C4

Technology Process of 1-Phenyl-5,6-dihydro-benzo[f]isoquinoline

There total 7 articles about 1-Phenyl-5,6-dihydro-benzo[f]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: N,N-Dimethyl-N'-[1-[1-(1-phenyl-vinyl)-3,4-dihydro-naphthalen-2-yl]-meth-(E)-ylidene]-hydrazine

: 131372-97-9
5,6-Dihydro-1-phenylbenzisoquinoline

Guidance literature:: In tetrahydrofuran; at 67 ℃;
DOI:10.1016/S0040-4039(00)97965-6

Reference yield:

: 117582-62-4
1-bromo-2-formyl-3,4-dihydronaphthalene

: 131372-97-9
5,6-Dihydro-1-phenylbenzisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 4-toluenesulfonic acid / diethyl ether / 3 h / Ambient temperature

With toluene-4-sulfonic acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)86333-X

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 131372-97-9
5,6-Dihydro-1-phenylbenzisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 1) PBr₃ / 1) CH₂Cl₂, 0 deg C, 1 h, 2) CH₂Cl₂, reflux, 1 h

2: 99 percent / 4-toluenesulfonic acid / diethyl ether / 3 h / Ambient temperature

With phosphorus tribromide; toluene-4-sulfonic acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)86333-X