3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal

Base Information

• Chemical Name: 3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal
• CAS No.: 3509-39-5
• Molecular Formula: C₁₄H₂₈N₂O₅S₂
• Molecular Weight: 368.519
• Mol file: 3509-39-5.mol

Synonyms:3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal;3,6-Di(acetylamino)-3,6-dideoxy-D-altrose diethyl dithioacetal

Chemical Property of 3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal

Chemical Property:

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Technology Process of 3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal

There total 3 articles about 3,6-Di(acetylamino)-3,6-dideoxy-D-altro-hexose diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3.6-Diacetamido-2.4.5-tri-O-acetyl-3.6-dideoxy-D-altrose-diethyldithioacetal (4157-10-2) → 3.6-Diacetamido-3.6-dideoxy-D-altrose-diethyldithioacetal (3509-39-5)

Guidance literature:

With ammonia; In methanol;

DOI:10.1021/jo01021a031

Reference yield:

→ N-[4-Acetylamino-1-(2,2-bis-ethylsulfanyl-1-hydroxy-ethyl)-2,3-dihydroxy-butyl]-acetamide (3509-39-5,63532-23-0)

Guidance literature:

Dithioacetal XX, Ammoniak, Methanol;

Reference yield:

→ N-[(1R,2S,3R)-4-Acetylamino-1-((R)-2,2-bis-ethylsulfanyl-1-hydroxy-ethyl)-2,3-dihydroxy-butyl]-acetamide (3509-39-5,63532-23-0)

Guidance literature:

Dithioacetal 9, NH3/MeOH;

upstream raw materials:

3.6-Diacetamido-2.4.5-tri-O-acetyl-3.6-dideoxy-D-altrose-diethyldithioacetal

Downstream raw materials:

3,6-Bis-(2,4-dinitro-anilino)-1,3,6-tridesoxy-D-altrit

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