1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol

Base Information

Chemical Name:1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol
CAS No.:213180-20-2
Molecular Formula:C₉H₁₈N₂O
Molecular Weight:170.255
Hs Code.:
DSSTox Substance ID:DTXSID50573552
Nikkaji Number:J1.225.147E
Wikidata:Q82462296
Mol file:213180-20-2.mol

Synonyms:213180-20-2;1,2,5,6-TETRAHYDRO-2,2,4,6,6-PENTAMETHYL-1-PYRIMIDINOL;SCHEMBL6552418;DTXSID50573552;AKOS006279763;2,2,4,6,6-Pentamethyl-5,6-dihydropyrimidin-1(2H)-ol

Suppliers and Price of 1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2,5,6-TETRAHYDRO-2,2,4,6,6-PENTAMETHYL-1-PYRIMIDINOL 95.00%
5MG
$ 500.47

Total 2 raw suppliers

Chemical Property of 1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol

Chemical Property:

Vapor Pressure:0.0174mmHg at 25°C
Boiling Point:235.3°C at 760 mmHg
Flash Point:96.1°C
PSA：35.83000
Density:1.01g/cm³
LogP:1.43040
XLogP3:0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:170.141913202
Heavy Atom Count:12
Complexity:219

Purity/Quality:

98%min ^*data from raw suppliers

1,2,5,6-TETRAHYDRO-2,2,4,6,6-PENTAMETHYL-1-PYRIMIDINOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC(N(C(C1)(C)C)O)(C)C

Technology Process of 1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol

There total 3 articles about 1,2,5,6-Tetrahydro-2,2,4,6,6-pentamethyl-1-pyrimidinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 213180-19-9
2,2,4,6,6-pentamethyl-1,2,5,6-tetrahdyro-pyridmidine-1-oxyl

: 213180-20-2
1-hydroxy-2,2,4,6,6-pentamethyl-1,2,5,6-tetrahydropyrimidine

Guidance literature:: With hydrazine; In diethyl ether;
DOI:10.1016/S0040-4039(99)02049-3

Reference yield: 36.0%

: 321862-22-0
2,2,4,4,6-pentamethyl-7-oxa-1,3-diaza-bicyclo[4.1.0]heptan-3-oxyl

: 213180-20-2
1-hydroxy-2,2,4,6,6-pentamethyl-1,2,5,6-tetrahydropyrimidine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1016/S0040-4039(00)01557-4

Reference yield:

: 556-72-9
2,2,4,4,6-pentamethyl-2,3,4,5,tetrahydropyrimidine

: 213180-20-2
1-hydroxy-2,2,4,6,6-pentamethyl-1,2,5,6-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / MCPBA / diethyl ether

2: 36 percent / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; 1: Oxidation / 2: Reduction;
DOI:10.1016/S0040-4039(00)01557-4