1-Triphenylenecarboxylic acid methyl ester

Base Information

Chemical Name:1-Triphenylenecarboxylic acid methyl ester
CAS No.:56909-16-1
Molecular Formula:C₂₀H₁₄O₂
Molecular Weight:286.33
Hs Code.:

Synonyms:1-Triphenylenecarboxylic acid methyl ester

Suppliers and Price of 1-Triphenylenecarboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1-Triphenylenecarboxylic acid methyl ester

Chemical Property:

Melting Point:150 °C (ethanol)
PSA：26.30000
LogP:4.93280

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 1-Triphenylenecarboxylic acid methyl ester

There total 2 articles about 1-Triphenylenecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1000071-27-1
methyl 2′-bromo-[1,1′-biphenyl]-2-carboxylate

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 56909-16-1
Triphenylen-carbonsaeure-(1)-methylester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cesium fluoride; tris-(o-tolyl)phosphine; In acetonitrile; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1039/c7tc02254a

Reference yield:

: 856644-86-5
4-Oxo-spiro-(cyclohexadien-(2,5)-1,9'-fluorenon)-carbonsaeure-⁽²⁾-methylester

: 56909-16-1
Triphenylen-carbonsaeure-(1)-methylester

Guidance literature:: Multistep reaction; (i) Al(OiPr)3, iPrOH, (ii) H₂SO₄, EtOH;

Reference yield:

: 56909-16-1
Triphenylen-carbonsaeure-(1)-methylester

: C₁₉H₁₀O

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / Inert atmosphere; Schlenk technique

2: Eaton’s reagent / 3 h / 80 °C / Inert atmosphere; Schlenk technique

With Eaton’s reagent; potassium hydroxide; In methanol;
DOI:10.1039/c7tc02254a