(1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester

Base Information

• Chemical Name: (1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester
• CAS No.: 6488-67-1
• Molecular Weight: 452.54
• Mol file: 6488-67-1.mol

Synonyms:(1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester;Desoxyandirobin

Chemical Property of (1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester

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Technology Process of (1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester

There total 2 articles about (1R,2R)-2-[(1R)-1α-(3-Furanyl)-3,5,6,7,8,8a-hexahydro-8aα-methyl-5-methylene-3-oxo-1H-2-benzopyran-6β-yl]-2,6,6-trimethyl-5-oxo-3-cyclohexene-1-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Deoxyandirobin (6488-67-1)

Guidance literature:

Andirobin, CrCl2;

Reference yield:

→ Anhydroangolesinsaeure-methylester, Desoxy-andirobin (6488-67-1)

Guidance literature:

Anhydroangolesinsaeure C26H30O6 (Syst. 2896), Diazomethan;

DOI:10.1039/j39660000944

Reference yield: 35.0%

deoxyandirobin (6488-67-1) → (1R,8aR)-1-Furan-3-yl-8a-methyl-5-methylene-6-((1S,5R,6R)-6,9,9-trimethyl-3-oxo-2-oxa-bicyclo[3.3.1]non-7-en-6-yl)-1,5,6,7,8,8a-hexahydro-isochromen-3-one (130877-15-5) + [(1R,2R,5R)-2-((1R,8aR)-1-Furan-3-yl-8a-methyl-5-methylene-3-oxo-3,5,6,7,8,8a-hexahydro-1H-isochromen-6-yl)-5-hydroxy-2,6,6-trimethyl-cyclohex-3-enyl]-acetic acid isopropyl ester (130877-21-3)

Guidance literature:

With isopropyl alcohol; aluminium; for 2h; Heating;

Downstream raw materials:

(1R,8aR)-1-Furan-3-yl-8a-methyl-5-methylene-6-((1S,5R,6R)-6,9,9-trimethyl-3-oxo-2-oxa-bicyclo[3.3.1]non-7-en-6-yl)-1,5,6,7,8,8a-hexahydro-isochromen-3-one

[(1R,2R,5R)-2-((1R,8aR)-1-Furan-3-yl-8a-methyl-5-methylene-3-oxo-3,5,6,7,8,8a-hexahydro-1H-isochromen-6-yl)-5-hydroxy-2,6,6-trimethyl-cyclohex-3-enyl]-acetic acid isopropyl ester

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