(3-Methoxynaphthalen-1-yl)boronic acid

Base Information

• Chemical Name: (3-Methoxynaphthalen-1-yl)boronic acid
• CAS No.: 219834-94-3
• Molecular Formula: C11H11BO3
• Molecular Weight: 202.01424
• Hs Code.: 2931900090
• Mol file: 219834-94-3.mol

Synonyms:(3-Methoxynaphthalen-1-yl)boronic acid;3-Methoxy-1-naphthaleneboronic acid

Chemical Property of (3-Methoxynaphthalen-1-yl)boronic acid

Chemical Property:

• Boiling Point: 424.6±47.0 °C(Predicted)
• PKA: 8.29±0.30(Predicted)
• PSA: 49.69000
• Density: 1.23±0.1 g/cm3(Predicted)
• LogP: 0.52820
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

(3-Methoxynaphthalen-1-yl)boronicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (3-Methoxynaphthalen-1-yl)boronic acid is a useful chemical for research.

Technology Process of (3-Methoxynaphthalen-1-yl)boronic acid

There total 1 articles about (3-Methoxynaphthalen-1-yl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-3-methoxy-naphthalene (5111-34-2) → (3- methoxynaphthalen- 1-yl)boronic acid (219834-94-3)

Guidance literature:

1-bromo-3-methoxy-naphthalene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 1h;

With Trimethyl borate; In diethyl ether; hexane; at -78 - 20 ℃;

With hydrogenchloride; In diethyl ether; hexane; water; at 20 ℃; for 0.75h;

DOI:10.1021/jo991011h

Reference yield:

2-amino-4-bromo-5-chloro-3-fluorobenzoic acid (1698027-17-6) + (3- methoxynaphthalen- 1-yl)boronic acid (219834-94-3) → 2-amino-5-chloro-3-fluoro-4-(3-methoxynaphthalen-1-yl)benzoic acid

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; at 100 ℃; for 21h;

Reference yield:

2-amino-4-bromo-5-chloro-3-fluorobenzamide + (3- methoxynaphthalen- 1-yl)boronic acid (219834-94-3) → 2-amino-5-chloro-3-fluoro-4-(3-methoxynaphthalen-1-yl)benzamide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; at 90 ℃; for 48h;

upstream raw materials:

1-bromo-3-methoxy-naphthalene

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