S-N,N,3-triMethylbutane-1,2-diaMine

Base Information

Chemical Name:S-N,N,3-triMethylbutane-1,2-diaMine
CAS No.:847696-16-6
Molecular Formula:C7H18N2
Molecular Weight:130.233
Hs Code.:2921290090
Mol file:847696-16-6.mol

Synonyms:S-N,N,3-triMethylbutane-1,2-diaMine;(2S)-N1,N1,3-TriMethyl-1,2-butanediaMine 2HCl

Suppliers and Price of S-N,N,3-triMethylbutane-1,2-diaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride
1 g
$ 1152.00

SynQuest Laboratories
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride
250 mg
$ 482.00

SynQuest Laboratories
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride
500 mg
$ 770.00

Apolloscientific
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride 97%
500mg
$ 698.00

Apolloscientific
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride 97%
250mg
$ 437.00

Apolloscientific
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride 97%
1g
$ 1044.00

Acrotein
(2S)-N1,N1,3-Trimethyl-1,2-butanediamine2HCl 97%
0.25g
$ 183.33

ACHEMBLOCK
(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride 95%
250MG
$ 215.00

Total 6 raw suppliers

Chemical Property of S-N,N,3-triMethylbutane-1,2-diaMine

Chemical Property:

Boiling Point:144.7±8.0 °C(Predicted)
PKA:9.76±0.13(Predicted)
PSA：29.26000
Density:0.836±0.06 g/cm3(Predicted)
LogP:1.23160

Purity/Quality:

99.0% ^*data from raw suppliers

(2S)-N1,N1,3-Trimethyl-1,2-butanediaminedihydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of S-N,N,3-triMethylbutane-1,2-diaMine

There total 5 articles about S-N,N,3-triMethylbutane-1,2-diaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154462-98-3
N,N-dimethyl-L-valinamide hydrochloride

: 847696-16-6,486414-51-1,773045-76-4
(S)-N¹,N¹,3-trimethylbutane-1,2-diamine

Guidance literature:: N,N-dimethyl-L-valinamide hydrochloride; With lithium aluminium tetrahydride; In tetrahydrofuran; Heating / reflux;

With sodium hydroxide; water; In tetrahydrofuran; ipa; for 2h;

Reference yield:

: 132393-07-8
(S)-tert-butyl (1-(dimethylamino)-3-methyl-1-oxobutan-2-yl)carbamate

: 847696-16-6,486414-51-1,773045-76-4
(S)-N¹,N¹,3-trimethylbutane-1,2-diamine

Guidance literature:: (S)-tert-butyl (1-(dimethylamino)-3-methyl-1-oxobutan-2-yl)carbamate; With acetyl chloride; In methanol; at 0 ℃;

With lithium aluminium tetrahydride; In tetrahydrofuran; Further stages.; Heating;
DOI:10.1021/ol702074a

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 847696-16-6,486414-51-1,773045-76-4
(S)-N¹,N¹,3-trimethylbutane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran / 0.33 h / -10 °C / Inert atmosphere

1.2: 24 h / -10 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 1.5 h / -15 °C / Inert atmosphere

3.1: hydrogenchloride / methanol; water / 3 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; chloroformic acid ethyl ester; In tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1021/ja401457h