cis-1-(Boc-aMino)-3-cyanocyclohexane, 97%

Base Information

• Chemical Name: cis-1-(Boc-aMino)-3-cyanocyclohexane, 97%
• CAS No.: 1198163-56-2
• Molecular Formula: C₁₂H₂₀N₂O₂
• Molecular Weight: 224.303
• Mol file: 1198163-56-2.mol

Synonyms:cis-1-(Boc-aMino)-3-cyanocyclohexane, 97%;tert-Butyl cis-4-cyanocyclohexylcarbamate

Chemical Property of cis-1-(Boc-aMino)-3-cyanocyclohexane, 97%

Chemical Property:

• PSA: 62.12000
• LogP: 2.98438

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl cis-4-cyanocyclohexylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cis-1-(Boc-aMino)-3-cyanocyclohexane, 97%

There total 7 articles about cis-1-(Boc-aMino)-3-cyanocyclohexane, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

→ tert-butyl (cis)-4-cyanocyclohexylcarbamate (1198163-56-2,1303968-12-8)

Guidance literature:

Reference yield: 68.6%

1,1-dimethylethyl [trans-4-(aminocarbonyl)cyclohexyl]carbamate (643067-91-8) → tert-butyl ((1r,4r)-4-cyanocyclohexyl)carbamate (873537-32-7,1198163-56-2,1303968-12-8)

Guidance literature:

With pyridine; trichlorophosphate; at 0 ℃; for 0.5h;

DOI:10.1021/jm300623u

Reference yield: 68.6%

trans-(4-carbamoyl-cyclohexyl)-carbamic acid tert-butyl ester → tert-butyl (trans)-4-cyanocyclohexylcarbamate (1198163-56-2,1303968-12-8)

Guidance literature:

With pyridine; trichlorophosphate; at 0 ℃;

upstream raw materials:

tert-butyl alcohol

1,1-dimethylethyl [trans-4-(aminocarbonyl)cyclohexyl]carbamate

trans-4-(tert-butoxycarbonylamino)cyclohexanoic acid

trans-4-(tert-butoxycarbonylamino)cyclohexane carboxylic acid

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