5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

Base Information

Chemical Name:5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one
CAS No.:53439-88-6
Molecular Formula:C9H11N3O
Molecular Weight:177.2
Hs Code.:2933990090
European Community (EC) Number:844-513-5
DSSTox Substance ID:DTXSID40354711
Nikkaji Number:J3.430.698B
Wikidata:Q82133054
ChEMBL ID:CHEMBL4128196
Mol file:53439-88-6.mol

Synonyms:53439-88-6;5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one;5-amino-1,3-dimethylbenzimidazol-2-one;110274-75-4;5-Amino-1,3-dimethyl-1,3-dihydro-benzoimidazol-2-one;5-Amino-1,3-dimethyl-1H-benzo[d]imidazol-2(3H)-one;5-amino-1,3-dimethyl-2,3-dihydro-1H-1,3-benzodiazol-2-one;MFCD00462960;5-AMINO-1,3-DIMETHYL-2-BENZIMIDAZOLINONE HYDROCHLORIDE;Oprea1_534372;Oprea1_685889;SCHEMBL1843229;CHEMBL4128196;DTXSID40354711;STK389035;AKOS000101250;BS-13863;SY031785;BB 0217057;CS-0067122;FT-0661746;FT-0692667;EN300-59698;C77632;A917931;5-Amino-1,3-dimethyl-1H-benzoimidazole-2(3H)-one;5-amino-1,3-dimethyl-1,3-dihydro-benzimidazol-2-on;5-amino-1,3-dimethyl-1,3-dihydrobenzimidazol-2-one;Z57834657;5-amino-1,3-dimethyl-1,3-dihydro-2H-1,3-benzimidazol-2-one;5-AMINO-1,3-DIMETHYL-1,3-DIHYDRO-2H-BENZO[D]IMIDAZOL-2-ONE;8TD

Suppliers and Price of 5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one
50mg
$ 45.00

Matrix Scientific
5-Amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one 97%
1g
$ 672.00

Crysdot
5-Amino-1,3-dimethyl-1H-benzo[d]imidazol-2(3H)-one 95+%
25g
$ 1782.00

Crysdot
5-Amino-1,3-dimethyl-1H-benzo[d]imidazol-2(3H)-one 95+%
10g
$ 941.00

Crysdot
5-Amino-1,3-dimethyl-1H-benzo[d]imidazol-2(3H)-one 95+%
5g
$ 554.00

Crysdot
5-Amino-1,3-dimethyl-1H-benzo[d]imidazol-2(3H)-one 95+%
1g
$ 251.00

ChemBridge Corporation
5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one 95%
250 mg
$ 99.00

ChemBridge Corporation
5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one 95%
10 g
$ 980.00

American Custom Chemicals Corporation
5-AMINO-1,3-DIMETHYL-2,3-DIHYDRO-1H-1,3-BENZODIAZOL-2-ONE 95.00%
5G
$ 1379.44

American Custom Chemicals Corporation
5-AMINO-1,3-DIMETHYL-2,3-DIHYDRO-1H-1,3-BENZODIAZOL-2-ONE 95.00%
2.5G
$ 1119.71

Total 10 raw suppliers

Chemical Property of 5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

Chemical Property:

Melting Point:135-136 °C(Solv: benzene (71-43-2))
Boiling Point:336.8±21.0 °C(Predicted)
PKA:5.86±0.20(Predicted)
PSA：52.95000
Density:1.271±0.06 g/cm3(Predicted)
LogP:1.04040
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:177.090211983
Heavy Atom Count:13
Complexity:231

Purity/Quality:

99%, ^*data from raw suppliers

5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)N)N(C1=O)C

Technology Process of 5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one

There total 10 articles about 5-amino-1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 43027-50-5
1,3-dimethyl-5-nitro-1,3-dihydro-2H-benzimidazol-2-one

: 53439-88-6
5-amino-1,3-dimethyl-1,3-dihydro-2H-benzo[d]imidazol-2-one

Guidance literature:: With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In ethanol; water;

Reference yield: 85.0%

: 5307-14-2,183870-67-9
2-nitro-1,4-phenylenediamine

: 616-38-6
carbonic acid dimethyl ester

: 53439-88-6
5-amino-1,3-dimethyl-1,3-dihydro-2H-benzo[d]imidazol-2-one

Guidance literature:: With copper(II) acetate monohydrate; In neat (no solvent); at 100 ℃; for 20h; under 7600.51 Torr; Autoclave; Inert atmosphere; Green chemistry;
DOI:10.1039/c4gc02408g