2-amino-3-bromo-5-nitrophenol

Base Information

Chemical Name:2-amino-3-bromo-5-nitrophenol
CAS No.:915156-09-1
Molecular Formula:C6H5BrN2O3
Molecular Weight:233.021
Hs Code.:
Mol file:915156-09-1.mol

Synonyms:2-amino-3-bromo-5-nitrophenol

Suppliers and Price of 2-amino-3-bromo-5-nitrophenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Amino-3-bromo-5-nitrophenol 97%
1g
$ 309.00

Chemcia Scientific
2-Amino-3-bromo-5-nitro-phenol 95%
5 G
$ 1035.00

Atlantic Research Chemicals
2-Amino-3-bromo-5-nitrophenol 95%
1gm:
$ 279.23

Alichem
2-Amino-3-bromo-5-nitrophenol
1g
$ 400.00

A1 Biochem Labs
2-Amino-3-bromo-5-nitrophenol 95%
10 g
$ 2500.00

Total 3 raw suppliers

Chemical Property of 2-amino-3-bromo-5-nitrophenol

Chemical Property:

Boiling Point:372.3±42.0 °C (760 mmHg)
PSA：92.07000
Density:1.971±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:2.74950

Purity/Quality:

98% ^*data from raw suppliers

2-Amino-3-bromo-5-nitrophenol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-amino-3-bromo-5-nitrophenol

There total 1 articles about 2-amino-3-bromo-5-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 121-88-0
5-Nitro-2-aminophenol

: 915156-09-1
2-amino-3-bromo-5-nitro-phenol

Guidance literature:: With bromine; In dichloromethane; at 0 - 20 ℃; for 0.75h;

Reference yield: 85.0%

: 915156-09-1
2-amino-3-bromo-5-nitro-phenol

: 116632-23-6
3-bromo-5-nitro-phenol

Guidance literature:: 2-amino-3-bromo-5-nitro-phenol; With sulfuric acid; In ethanol; for 0.5h; Heating / reflux;

With sodium nitrite; In ethanol; for 1h; Heating / reflux;

Reference yield:

: 915156-09-1
2-amino-3-bromo-5-nitro-phenol

: 1372548-00-9
1-[5-benzyloxy-7-(2-pyridyl)-1,3-benzothiazol-2-yl]-3-ethyl-urea

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; sodium nitrite / ethanol / 3 h / -10 - 55 °C / Reflux

2.1: potassium carbonate / [⁽²⁾H₆]acetone / 3.25 h / 20 °C / Reflux

3.1: tin(II) chloride dihdyrate / tetrahydrofuran / 3 h / Reflux

4.1: [⁽²⁾H₆]acetone / 0.75 h / 20 °C

5.1: water; sodium hydroxide / tetrahydrofuran / 20 - 70 °C

6.1: bromine / acetonitrile / 1 h / 0 - 20 °C

6.2: 0.5 h / 5 - 10 °C / pH 10 - 12

7.1: 1,4-dioxane / 80 - 85 °C

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tin(II) chloride dihdyrate; sulfuric acid; water; bromine; potassium carbonate; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; [⁽²⁾H₆]acetone; ethanol; N,N-dimethyl-formamide; acetonitrile; 8.1: |Stille Cross Coupling;