Icosanedioic acid bis(2,3-dihydroxypropyl) ester

Base Information

• Chemical Name: Icosanedioic acid bis(2,3-dihydroxypropyl) ester
• CAS No.: 75569-35-6
• Molecular Formula: C₂₆H₅₀O₈
• Molecular Weight: 490.678
• Mol file: 75569-35-6.mol

Synonyms:Icosanedioic acid bis(2,3-dihydroxypropyl) ester

Chemical Property of Icosanedioic acid bis(2,3-dihydroxypropyl) ester

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Icosanedioic acid bis(2,3-dihydroxypropyl) ester

There total 2 articles about Icosanedioic acid bis(2,3-dihydroxypropyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

C32H58O8 → C26H50O8 (75569-35-6) + C29H54O8

Guidance literature:

With water; acetic acid; at 50 ℃; for 0.416667h;

DOI:10.1016/j.tet.2013.11.021

Reference yield:

C17H30O4 → C26H50O8 (75569-35-6) + C29H54O8

Guidance literature:

Multi-step reaction with 3 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 760.05 Torr

3: water; acetic acid / 0.42 h / 50 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; palladium 10% on activated carbon; water; hydrogen; acetic acid; In dichloromethane; ethyl acetate;

DOI:10.1016/j.tet.2013.11.021