11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-

Base Information

Chemical Name:11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-
CAS No.:127040-49-7
Molecular Formula:C22H15 Cl N2
Molecular Weight:342.8209
Hs Code.:
DSSTox Substance ID:DTXSID00155382
Wikidata:Q83023285
Mol file:127040-49-7.mol

Synonyms:BRN 4266020;11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-;3-Chloro-11-benzylpyrido(3,2-a)carbazole;127040-49-7;3-Chloro-11-(phenylmethyl)-11H-pyrido(3,2-a)carbazole;C22H15ClN2;C22-H15-Cl-N2;DTXSID00155382;LS-133278

Suppliers and Price of 11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-

Chemical Property:

Vapor Pressure:4.52E-13mmHg at 25°C
Boiling Point:571.5°Cat760mmHg
Flash Point:299.4°C
Density:1.27g/cm³
XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:342.0923762
Heavy Atom Count:25
Complexity:463

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN2C3=CC=CC=C3C4=C2C5=C(C=C4)N=C(C=C5)Cl

Technology Process of 11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)-

There total 3 articles about 11H-Pyrido(3,2-a)carbazole, 3-chloro-11-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 127040-42-0
11H-3-chloropyrido<3,2-a>carbazole

: 100-44-7
benzyl chloride

: 127040-49-7
3-chloro-11-benzylpirydo<3,2-a>carbazole

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; for 6h;
DOI:10.1007/BF00764806

Reference yield:

: 127040-41-9
11H-3-oxo-3,4-dihydropyrido<3,2-a>carbazole

: 127040-49-7
3-chloro-11-benzylpirydo<3,2-a>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / POCl₃, Et₃N*HCl / 1 h / Heating

2: 64 percent / KOH / dimethylsulfoxide / 6 h

With potassium hydroxide; triethylamine hydrochloride; trichlorophosphate; In dimethyl sulfoxide;
DOI:10.1007/BF00764806

Reference yield:

: 127040-37-3
11H-3-oxo-3,4,5,6-tetrahydropyrido<3,2-a>carbazole

: 127040-49-7
3-chloro-11-benzylpirydo<3,2-a>carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / chloranil / benzene / 2 h / Heating

2: 96 percent / POCl₃, Et₃N*HCl / 1 h / Heating

3: 64 percent / KOH / dimethylsulfoxide / 6 h

With potassium hydroxide; triethylamine hydrochloride; chloranil; trichlorophosphate; In dimethyl sulfoxide; benzene;
DOI:10.1007/BF00764806