2-o-Tolyl-ethanesulfonyl chloride

Base Information

Chemical Name:2-o-Tolyl-ethanesulfonyl chloride
CAS No.:728919-61-7
Molecular Formula:C₉H₁₁ClO₂S
Molecular Weight:218.704
Hs Code.:
European Community (EC) Number:673-804-8
DSSTox Substance ID:DTXSID30375278
Wikidata:Q82163807
Mol file:728919-61-7.mol

Synonyms:728919-61-7;2-o-Tolyl-ethanesulfonyl chloride;2-(2-methylphenyl)ethanesulfonyl Chloride;2-o-tolylethanesulfonyl chloride;2-(o-tolyl)Ethanesulfonyl chloride;3-AMINO-OCTANOICACID;DTXSID30375278;2-(o-tolyl)Ethanesulfonylchloride;AKOS006222718;2-(O-tolyl)ethane-1-sulfonyl chloride;2-?Methylbenzeneethanesulfony?l chloride;CS-0281927;FT-0760516;2-(2-methylphenyl)ethane-1-sulfonyl chloride;EN300-272543

Suppliers and Price of 2-o-Tolyl-ethanesulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-(o-tolyl)Ethanesulfonylchloride 95+%
1g
$ 583.00

CHESS?
MC000647:2-o-Tolyl-ethanesulfonylchloride 97
5 g
$ 900.00

American Custom Chemicals Corporation
2-O-TOLYLETHANESULFONYL CHLORIDE 95.00%
1G
$ 1280.66

AHH
2-o-Tolylethanesulfonylchloride 98%
1g
$ 280.00

Total 5 raw suppliers

Chemical Property of 2-o-Tolyl-ethanesulfonyl chloride

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:218.0168285
Heavy Atom Count:13
Complexity:243

Purity/Quality:

98%min ^*data from raw suppliers

2-(o-tolyl)Ethanesulfonylchloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1CCS(=O)(=O)Cl

Technology Process of 2-o-Tolyl-ethanesulfonyl chloride

There total 1 articles about 2-o-Tolyl-ethanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 16793-90-1
1-(2-bromoethyl)-2-methylbenzene

: 728919-61-7
2-(2-methylphenyl)ethanesulfonyl chloride

Guidance literature:: 1-(2-bromoethyl)-2-methylbenzene; With potassium thioacetate; In acetonitrile; at 0 - 20 ℃; for 1h;

With hydrogenchloride; sodium chlorite; In water; acetonitrile; for 0.666667h;
DOI:10.1016/j.bmc.2017.05.040

Reference yield:

: 728919-61-7
2-(2-methylphenyl)ethanesulfonyl chloride

: N-(2-amino-5-chlorophenyl)-2-(2-methylphenyl)ethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 0.02 h

2: hydrogenchloride; zinc / water; ethanol / 1 h / 0 - 100 °C

With hydrogenchloride; sodium hydride; zinc; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2017.05.040

Reference yield:

: 728919-61-7
2-(2-methylphenyl)ethanesulfonyl chloride

: 6-chloro-1-{[2-(2-methylphenyl)ethyl]sulfonyl}-1,3-dihydro-2H-benzimidazol-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 0.02 h

2: hydrogenchloride; zinc / water; ethanol / 1 h / 0 - 100 °C

3: hydrogenchloride / water; toluene / 4 h / 100 °C

With hydrogenchloride; sodium hydride; zinc; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2017.05.040