Tryptindane

Base Information

• Chemical Name: Tryptindane
• CAS No.: 14838-97-2
• Molecular Formula: C₂₃H₁₈
• Molecular Weight: 294.396
• Mol file: 14838-97-2.mol

Synonyms:9H,10H-4b,9a-(o-Benzenomethano)indeno[1,2-a]indene(8CI); Triptindane

Chemical Property of Tryptindane

Chemical Property:

• PSA: 0.00000
• LogP: 4.67570

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tryptindane

There total 5 articles about Tryptindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C65H42N24O6 (106116-57-8) → Triptindan (14838-97-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; dichloromethane; for 24h; under 760 Torr; Ambient temperature;

Reference yield: 76.0%

Triptindan-9-one (134939-91-6) → Triptindan (14838-97-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 24h; under 2700.2 Torr; Ambient temperature;

DOI:10.1021/jo00015a034

Reference yield:

1H-indene-1,3(2H)-dione (606-23-5) → Triptindan (14838-97-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / KF, Celite / acetonitrile

2: 91 percent / polyphosphoric acid (PPA) / 120 °C / 12 - 60h

3: 76 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 2700.2 Torr / Ambient temperature

With potassium fluoride; PPA; Polyphosphoric acid (PPA); Celite; hydrogen; palladium on activated charcoal; In ethanol; acetonitrile;

DOI:10.1021/jo00015a034

upstream raw materials:

Triptindan-9-one

C₆₅H₄₂N₂₄O₆

1H-indene-1,3(2H)-dione

2,2-dibenzyl-2,3-dihydro-1H-indene-1,3-dione