2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one

Base Information

Chemical Name:2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one
CAS No.:13212-62-9
Molecular Formula:C₁₂H₁₅NO₃
Molecular Weight:221.256
Hs Code.:
Mol file:13212-62-9.mol

Synonyms:2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one;2-Butyl-4-hydroxy-2H-1,4-benzoxazin-3(4H)-one

Suppliers and Price of 2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one

Chemical Property:

Boiling Point:360.3±45.0 °C(Predicted)
PKA:8.05±0.40(Predicted)
Density:1.212±0.06 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

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Pictogram(s):
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Technology Process of 2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one

There total 2 articles about 2-Butyl-4-hydroxy-2,3-dihydro-4H-1,4-benzooxazine-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13212-59-4
C₁₄H₁₉NO₅

: 13212-62-9
2-butyl-4-hydroxy-2H-benzo[b][1,4]oxazin-3(4H)-one

Guidance literature:: With sodium tetrahydroborate; palladium 10% on activated carbon; In 1,4-dioxane; water; for 1h;
DOI:10.1021/jf802735m

Reference yield:

: 615-96-3
Ethyl 2-bromohexanoate

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 13212-62-9
2-butyl-4-hydroxy-2H-benzo[b][1,4]oxazin-3(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 1 h

2: palladium 10% on activated carbon; sodium tetrahydroborate / water; 1,4-dioxane

With sodium tetrahydroborate; palladium 10% on activated carbon; potassium hydroxide; In 1,4-dioxane; ethanol; water;
DOI:10.1080/00397911.2018.1554146