Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI)

Base Information

Chemical Name:Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI)
CAS No.:87001-64-7
Molecular Formula:C11H19N
Molecular Weight:165.279
Hs Code.:
Mol file:87001-64-7.mol

Synonyms:Cyclohexanecarbonitrile,2-methyl-5-(1-methylethyl)-,[1R-(1alpha,2alpha,5bta)]-(9CI);Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI);Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5b

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI)

Chemical Property:

PSA：23.79000
LogP:3.21838

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI)

There total 2 articles about Cyclohexanecarbonitrile, 2-methyl-5-(1-methylethyl)-, [1R-(1alpha,2alpha,5ba)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 151-50-8
potassium cyanide

: 5055-99-2
(+)-(1S,2S,5S)-carvomenthyl tosylate

: 5056-00-8
(3S,6R)-3-methyl-6-(1-methylethyl)cyclohexene

: 1845-59-6
(1S,2S,4S)-(+)-carvomenthol

: 5563-78-0
(-)neocarvomenthol

: 499-94-5,5502-88-5,34363-01-4
(S)-carvomenthene

: 87001-64-7
(-)neocarvomenthyl carbonitrile

Guidance literature:: In dimethyl sulfoxide; at 110 - 115 ℃; for 6.5h; Product distribution; var. solvents;

Reference yield:

: 151-50-8
potassium cyanide

: 5055-99-2
(+)-(1S,2S,5S)-carvomenthyl tosylate

: 5056-00-8
(3S,6R)-3-methyl-6-(1-methylethyl)cyclohexene

: 5563-78-0
(-)neocarvomenthol

: 499-94-5,5502-88-5,34363-01-4
(S)-carvomenthene

: 87001-64-7
(-)neocarvomenthyl carbonitrile

Guidance literature:: In dimethyl sulfoxide; at 110 - 115 ℃; for 6.5h;

Reference yield:

: 87001-64-7
(-)neocarvomenthyl carbonitrile

: 87001-66-9
(+)(1S,2S,4S) 1-methyl-4-isopropyl-cyclohexyl-2-carboamide

Guidance literature:: Multi-step reaction with 3 steps

1: 12.6 g / KOH / ethane-1,2-diol / 20 h / Heating

2: SOCl₂ / 5 h / Heating

3: 4.2 g / aq. NH₃

With potassium hydroxide; ammonium hydroxide; thionyl chloride; In ethylene glycol;