alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)

Base Information

Chemical Name:alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)
CAS No.:495379-04-9
Molecular Formula:C11H20O4
Molecular Weight:216.27
Hs Code.:
Mol file:495379-04-9.mol

Synonyms:alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)

Suppliers and Price of alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)

Chemical Property:

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Technology Process of alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI)

There total 2 articles about alpha-D-erythro-Hexopyranoside,ethyl2,3-dideoxy-4-O-(1Z)-1-propenyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 495379-03-8
ethyl 4-O-allyl-6-O-tert-butyldimethylsilyl-2,3-dideoxy-α-D-erythro-hexopyranoside

: 495379-04-9
ethyl 2,3-dideoxy-(Z)-4-O-propenyl-α-D-erythro-hexopyranoside

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 50 ℃; for 2h;
DOI:10.1016/S0008-6215(02)00139-8

Reference yield:

: ethyl 6-O-tert-butyldimethylsilyl-2,3-dideoxy-α-D-erythro-hexopyranoside

: 495379-04-9
ethyl 2,3-dideoxy-(Z)-4-O-propenyl-α-D-erythro-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOH; Bu₄NBr / toluene

2: t-BuOK / dimethylsulfoxide / 2 h / 50 °C

With potassium hydroxide; potassium tert-butylate; tetrabutylammomium bromide; In dimethyl sulfoxide; toluene;
DOI:10.1016/S0008-6215(02)00139-8