(9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan

Base Information

• Chemical Name: (9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan
• CAS No.: 23979-17-1
• Molecular Formula: C19H21NO3
• Molecular Weight: 311.381
• Mol file: 23979-17-1.mol

Synonyms:(9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan

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Chemical Property of (9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan

Chemical Property:

• Melting Point: 193 - 194 °C
• Boiling Point: 467.6±45.0 °C(Predicted)
• PKA: 7.46±0.40(Predicted)
• PSA: 30.93000
• Density: 1.30±0.1 g/cm3(Predicted)
• LogP: 2.36240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan

There total 5 articles about (9S,13R)-6,7,8,14-Tetradehydro-4,5β-epoxy-3,6-dimethoxy-17-methylmorphinan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (+-)-thebaine (115-37-7,23979-17-1,23979-19-3)

Guidance literature:

Brom-ketal 16, (CH3)3CO-K+;

DOI:10.1021/jm00232a001

Reference yield:

→ 4,5α-epoxy-3,6-dimethoxy-17-methyl-morphina-6,8(14)-diene (115-37-7,23979-17-1,23979-19-3)

Guidance literature:

Biochemisch aus Reticulin;

DOI:10.1021/ja01075a043

Reference yield:

→ 4,5-epoxy-3,6-dimethoxy-17-methyl-morphina-6,8(14)-diene (115-37-7,23979-17-1,23979-19-3)

Guidance literature:

Salutaridinol, NaBH4, SOCl2, NaOH;

Downstream raw materials:

(2-hydroxyethyl)(methyl)amine

3,6-Dimethoxy-4-acetoxyphenanthrene

6-methoxy-4-(2-methylamino-ethyl)-phenanthrene-1,5-diol

4-hydroxy-3-methoxy-17-methyl-14,15-cyclo-13,15-seco-morphin-5⁽¹³⁾-en-6-one