9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine

Base Information

• Chemical Name: 9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine
• CAS No.: 935772-63-7
• Molecular Formula: C₁₂H₁₁Cl₂N
• Molecular Weight: 240.132
• Mol file: 935772-63-7.mol

Synonyms:9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine

Chemical Property of 9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine

Chemical Property:

• Boiling Point: 345.4±42.0 °C(Predicted)
• PKA: 3.86±0.20(Predicted)
• PSA: 26.02000
• Density: 1.421±0.06 g/cm3(Predicted)
• LogP: 4.51380
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

9-(Dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalen-5-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 9-(Dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalen-5-amine is used in fungicidal compositions useful in controlling rust diseases of soyabean plant.

Technology Process of 9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine

There total 21 articles about 9-(DichloroMethylene)-1,2,3,4-tetrahydro-1,4-Methanonaphthalen-5-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.9%

N-(1,2,3,4-tetrahydro-1,4-methylenenaphthalene-9-dichloromethylen-5-yl)phthalimide → 9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalene-5-amine (935772-63-7)

Guidance literature:

With hydrazine hydrate; In ethanol; at 90 ℃; for 3.5h; Reagent/catalyst;

Reference yield: 85.1%

C20H13Cl2NO2 → C12H11Cl2N (935772-63-7)

Guidance literature:

With methylamine; In ethanol; water; at 90 ℃; for 3.5h; Reagent/catalyst;

Reference yield: 79.0%

5-bromo-9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalene (1345203-43-1) → 9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalene-5-amine (935772-63-7)

Guidance literature:

With ammonia; sodium t-butanolate; (R)-1-[(S_P)-2-(dicyclohexylphosphino)ferrocenyl]ethyldi-tert-butylphosphine; palladium diacetate; In Dimethyl ether; at 105 ℃; for 32h; under 7875.79 - 12001.2 Torr; Autoclave; Inert atmosphere;

upstream raw materials:

5-bromo-9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalene

[2,3]epoxy-5-nitro-1,2,3,4-tetrahydro-1,4-methanonaphthalene

5-amino-1,2,3,4-tetrahydro-1,4-methanonaphthalene-9-ol

6-nitroanthranilic acid

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