S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol

Base Information

• Chemical Name: S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol
• CAS No.: 1228600-98-3
• Molecular Formula: C34H28F6O2
• Molecular Weight: 582.5753392
• Mol file: 1228600-98-3.mol

Synonyms:S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol

Chemical Property of S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol

Chemical Property:

• PSA: 40.46000
• LogP: 9.89400

Purity/Quality:

99% ^*data from raw suppliers

(S)-3,3'-Bis(4-(trifluoromethyl)phenyl)-5,5',6,6',7,7',8,8'-octahydro-[1,1'-binaphthalene]-2,2'-diol 98% ^*data from reagent suppliers

Safty Information:

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Technology Process of S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol

There total 1 articles about S-3,3'-bis[4-(trifluoroMethyl)phenyl]-5,5',6,6',7,7',8,8'-octahydro-[1,1'-Binaphthalene]-2,2'-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

→ (R)-3,3'-bis(4-trifluoromethylphenyl)-2,2'-dihydroxy-5,5',6,6',7,7',8,8'-octahydro-1,1'-dinaphthyl (1228600-98-3,791616-69-8)

Guidance literature:

Reference yield: 55.0%

(R)-3,3'-bis(4-trifluoromethylphenyl)-2,2'-dihydroxy-5,5',6,6',7,7',8,8'-octahydro-1,1'-dinaphthyl (1228600-98-3,791616-69-8) + (1S,1'S)-bis(1-phenylethyl)amine (21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1,10024-74-5) → N,N-bis((S)-1-phenylethyl)-2,6-bis(4-(trifluoromethyl)phenyl)-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine

Guidance literature:

(R)-3,3'-bis(4-trifluoromethylphenyl)-2,2'-dihydroxy-5,5',6,6',7,7',8,8'-octahydro-1,1'-dinaphthyl; With triethylamine; phosphorus trichloride; In tetrahydrofuran; at 0 - 70 ℃; Schlenk technique; Inert atmosphere;

(1S,1'S)-bis(1-phenylethyl)amine; In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.1c06144

Reference yield: 52.0%

C34H28F6O2 (1228600-98-3,791616-69-8) + (R,R)-N,N-bis-(1-phenylethyl)amine (10024-74-5,21003-56-5,21003-57-6,23294-41-9,42287-48-9,56210-72-1) → (11bS)-N,N-bis((R)-1-phenylethyl)-2,6-bis(4-(trifluoromethyl)phenyl)-8,9,10,11,12,13,14,15-octahydrodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine

Guidance literature:

C₃₄H₂₈F₆O₂; With triethylamine; phosphorus trichloride; In tetrahydrofuran; at 0 - 70 ℃; Schlenk technique; Inert atmosphere;

(R,R)-N,N-bis-(1-phenylethyl)amine; In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.1c06144

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