Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)
CAS No.:166271-53-0
Molecular Formula:C₈H₁₇NO₃
Molecular Weight:175.228
Hs Code.:
Mol file:166271-53-0.mol

Synonyms:Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)

Suppliers and Price of Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI)

There total 2 articles about Carbamic acid, (3-hydroxy-1,1-dimethylbutyl)-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.1%

: 65330-08-7
Methyl-N-(1,1-dimethyl-3-oxobutyl)-carbamat

: 166271-53-0
methyl N-(2-methyl-3-hydroxybutyl-1)carbamate

Guidance literature:: With sodium tetrahydroborate; sodium dihydrogenphosphate; camphor-10-sulfonic acid; In methanol; water; for 1h;
DOI:10.1007/BF01165021

Reference yield:

: 18920-76-8
1-dimethyl-3-oxo-butane hydrochloride

: 166271-53-0
methyl N-(2-methyl-3-hydroxybutyl-1)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / diethyl ether / 0.5 h / 20 °C

2: 92 percent / aq. NaBH₄ / methanol; aq. phosphate buffer / 1 h

With sodium hydroxide; sodium tetrahydroborate; In methanol; phosphate buffer; diethyl ether;
DOI:10.1023/A:1011660706513

Reference yield: 87.0%

: 166271-53-0
methyl N-(2-methyl-3-hydroxybutyl-1)carbamate

: 27830-77-9
4,4,6-trimethyl-tetrahydro-[1,3]oxazin-2-one

Guidance literature:: methyl N-(2-methyl-3-hydroxybutyl-1)carbamate; With sodium tetrahydroborate; In ethanol;

With sodium hydroxide; In ethanol;
DOI:10.1023/A:1011660706513