CHEMBRDG-BB 6624595

Base Information

• Chemical Name: CHEMBRDG-BB 6624595
• CAS No.: 108129-37-9
• Molecular Formula: C₈H₈N₂O₂
• Molecular Weight: 164.164
• Hs Code.: 2934999090
• Mol file: 108129-37-9.mol

Synonyms:CHEMBRDG-BB 6624595;4-AMINO-6-METHYLFURO[3,4-C]PYRIDIN-3(1H)-ONE;AKOS BB816;4-amino-6-methylfuro[3,4-c]pyridin-3(1H)-one(SALTDATA: FREE)

Chemical Property of CHEMBRDG-BB 6624595

Chemical Property:

• Vapor Pressure: 4.03E-07mmHg at 25°C
• Boiling Point: 415.7°C at 760 mmHg
• Flash Point: 205.2°C
• PSA: 65.21000
• Density: 1.393g/cm³
• LogP: 1.22380

Purity/Quality:

97% ^*data from raw suppliers

4-Amino-6-methylfuro[3,4-c]pyridin-3(1H)-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 6624595

There total 3 articles about CHEMBRDG-BB 6624595 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-4-methoxymethyl-6-methyl-nicotinic acid amide (98961-02-5) → 4-amino-6-methyl-1H-furo[3,4-c]pyridin-3-one (108129-37-9)

Guidance literature:

With sulfuric acid;

DOI:10.1021/ja01519a043

Reference yield:

4-methoxymethyl-6-methyl-1,2-dihydro-pyrazolo[3,4-b]pyridin-3-one (116080-96-7) → 4-amino-6-methyl-1H-furo[3,4-c]pyridin-3-one (108129-37-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; ethanol

2: aqueous H₂SO₄

With ethanol; sulfuric acid; nickel;

DOI:10.1021/ja01519a043

Reference yield:

1-methoxypentane-2,4-dione (6290-50-2) → 4-amino-6-methyl-1H-furo[3,4-c]pyridin-3-one (108129-37-9)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH solution

2: Raney nickel; ethanol

3: aqueous H₂SO₄

With sodium hydroxide; ethanol; sulfuric acid; nickel;

DOI:10.1021/ja01519a043

upstream raw materials:

2-amino-4-methoxymethyl-6-methyl-nicotinic acid amide

4-methoxymethyl-6-methyl-1,2-dihydro-pyrazolo[3,4-b]pyridin-3-one

1-methoxypentane-2,4-dione

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