N-(furan-2-ylmethyl)prop-2-en-1-amine

Base Information

• Chemical Name: N-(furan-2-ylmethyl)prop-2-en-1-amine
• CAS No.: 53175-33-0
• Molecular Formula: C8H11NO
• Molecular Weight: 137.181
• Hs Code.: 2932190090
• DSSTox Substance ID: DTXSID50406018
• Nikkaji Number: J1.543.993I
• Wikidata: Q82210851
• Mol file: 53175-33-0.mol

Synonyms:53175-33-0;N-(furan-2-ylmethyl)prop-2-en-1-amine;N-(2-FURYLMETHYL)-2-PROPEN-1-AMINE;(furan-2-ylmethyl)(prop-2-en-1-yl)amine;CHEMBRDG-BB 9071357;MFCD07410484;allylfurfurylamine;[(furan-2-yl)methyl](prop-2-en-1-yl)amine;N-Allyl-2-furanmethanamine;SCHEMBL7445493;DTXSID50406018;AKOS000224060;N-[(Furan-2-yl)methyl]prop-2-en-1-amine;FT-0761163;EN300-111558

Chemical Property of N-(furan-2-ylmethyl)prop-2-en-1-amine

Chemical Property:

• Vapor Pressure: 0.708mmHg at 25°C
• Boiling Point: 185.1°C at 760 mmHg
• Flash Point: 65.8°C
• PSA: 25.17000
• Density: 0.966g/cm³
• LogP: 1.94610
• XLogP3: 1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 137.084063974
• Heavy Atom Count: 10
• Complexity: 103

Purity/Quality:

NLT 98% ^*data from raw suppliers

(furan-2-ylmethyl)(prop-2-en-1-yl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCNCC1=CC=CO1

Technology Process of N-(furan-2-ylmethyl)prop-2-en-1-amine

There total 7 articles about N-(furan-2-ylmethyl)prop-2-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

Allyl-[1-furan-2-yl-meth-(Z)-ylidene]-amine → N-(2-furylmethyl)-N-(prop-2-en-1-yl)amine (53175-33-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 5h;

DOI:10.1002/1099-0690(200105)2001:10<1845::AID-EJOC1845>3.0.CO;2-I

Reference yield: 81.0%

allyl-furfurylidene-amine (69374-42-1) → N-(2-furylmethyl)-N-(prop-2-en-1-yl)amine (53175-33-0)

Guidance literature:

allyl-furfurylidene-amine; With C₂₁H₃₉NPPd^(1-)*C₂F₃O₂^(1-); phenylsilane; In chloroform-d1; at 40 ℃; for 6h; Glovebox; Sealed tube;

With water; In chloroform-d1; regioselective reaction; Sealed tube; Glovebox;

DOI:10.1039/c5cy01859e

Reference yield: 80.0%

furfural (98-01-1) + 1-amino-2-propene (107-11-9,30551-89-4) → N-(2-furylmethyl)-N-(prop-2-en-1-yl)amine (53175-33-0)

Guidance literature:

furfural; 1-amino-2-propene; In ethanol; at 22 ℃; for 1h;

With sodium tetrahydroborate; at 0 - 22 ℃; for 17h;

DOI:10.1002/anie.201913125

upstream raw materials:

furan-2-ylmethanamine

allyl bromide

furfural

allyl-furfurylidene-amine

Downstream raw materials:

isoindoline