ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate

Base Information

• Chemical Name: ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate
• CAS No.: 76782-45-1
• Molecular Formula: C14H15ClO4
• Molecular Weight: 283
• Mol file: 76782-45-1.mol

Synonyms:ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate

Chemical Property of ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate

Chemical Property:

• Melting Point: 93 - 94 °C
• PSA: 77.51000
• LogP: 2.00420

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate

There total 1 articles about ethyl 6-(4-chlorophenyl)-4,6-dioxohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4'-chlorophenyl)-1,3-butanedione (6302-55-2) + oxalic acid diethyl ester (95-92-1) → ethyl 6-(4-chlorophenyl)-2,4,6-trioxohexanoate (76782-45-1)

Guidance literature:

In 1,2-dimethoxyethane; mineral oil;

Reference yield:

ethyl 6-(4-chlorophenyl)-2,4,6-trioxohexanoate (76782-45-1) → 6-(4-chlorophenyl)-4-oxo-4H-pyrane-2-carboxylic acid (76781-93-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane;

Reference yield:

ethyl 6-(4-chlorophenyl)-2,4,6-trioxohexanoate (76782-45-1) → ethyl 6-(4-chlorophenyl)-4-oxo-4H-pyran-2-carboxylate (76781-74-3)

Guidance literature:

In sulfuric acid;

upstream raw materials:

1-(4'-chlorophenyl)-1,3-butanedione

oxalic acid diethyl ester

Downstream raw materials:

ethyl 6-(4-chlorophenyl)-4-oxo-4H-pyran-2-carboxylate

6-(4-chlorophenyl)-4-oxo-4H-pyrane-2-carboxylic acid

Refernces