4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid

Base Information

• Chemical Name: 4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid
• CAS No.: 1401343-31-4
• Molecular Formula: C₃₃H₃₀O₉
• Molecular Weight: 570.596

Synonyms:4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid

Chemical Property of 4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

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Technology Process of 4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid

There total 2 articles about 4,4',4''-(((2,4,6-triMethylbenzene-1,3,5-triyl)tris(Methylene))tris(oxy))tribenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene (21988-87-4) + methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → 4,4′-(((5-((4-(hydroxy-l2-methoxy)phenoxy)methyl)-2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzoic acid (1401343-31-4)

Guidance literature:

methyl 4-hydroxylbenzoate; With sodium hydroxide; In dimethyl sulfoxide; at 75 ℃; for 1h;

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene; In dimethyl sulfoxide; at 75 ℃; for 24h;

DOI:10.1002/zaac.201300677

Reference yield:

C36H36O9 → 4,4′-(((5-((4-(hydroxy-l2-methoxy)phenoxy)methyl)-2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzoic acid (1401343-31-4)

Guidance literature:

With sodium hydroxide;

DOI:10.1134/S0022476620060190

Reference yield: 35.0%

magnesium(II) nitrate hexahydrate + N,N-dimethyl acetamide (127-19-5,116057-81-9) + 4,4′-(((5-((4-(hydroxy-l2-methoxy)phenoxy)methyl)-2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzoic acid (1401343-31-4) + water (7732-18-5) → [Mg4(TCMTB)2(OAc)2(DMA)2(H2O)3]n

Guidance literature:

at 120 ℃; for 120h; Autoclave; High pressure;

DOI:10.1039/c6ce01821a

upstream raw materials:

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene

methyl 4-hydroxylbenzoate

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