N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE

Base Information

• Chemical Name: N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE
• CAS No.: 123098-38-4
• Molecular Formula: C₁₃H₁₁ClN₂O
• Molecular Weight: 246.696
• Hs Code.: 2924299090
• Mol file: 123098-38-4.mol

Synonyms:N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE;AKOS BB-8152;LABOTEST-BB LT00511991;ART-CHEM-BB B025198;ASISCHEM T31117;OTAVA-BB 1166858

Chemical Property of N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE

Chemical Property:

• PSA: 55.12000
• LogP: 3.82870

Purity/Quality:

98%min ^*data from raw suppliers

N-(4-Aminophenyl)-3-chlorobenzamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE

There total 8 articles about N-(4-AMINOPHENYL)-3-CHLOROBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.8%

N-(4-nitrophenyl)-3-chlorophenyl carboxamide (71267-16-8) → N-(4-aminophenyl)-3-chlorophenyl carboxamide (123098-38-4)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; for 2h; Reflux;

Reference yield: 67.5%

→ N-(4-aminophenyl)-3-chlorophenyl carboxamide (123098-38-4)

Guidance literature:

With acetic acid; zinc; In methanol; water; for 1h; Reflux;

Reference yield:

[4-(3-Chloro-benzoylamino)-phenyl]-carbamic acid tert-butyl ester → N-(4-aminophenyl)-3-chlorophenyl carboxamide (123098-38-4)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2019.126711

upstream raw materials:

4-nitro-aniline

m-Chlorobenzoyl chloride

N-(4-nitrophenyl)-3-chlorophenyl carboxamide

3-chlorobenzoate

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