t-Butyl (5-iodopyridin-3-yl)carbamate

Base Information

• Chemical Name: t-Butyl (5-iodopyridin-3-yl)carbamate
• CAS No.: 857266-59-2
• Molecular Formula: C₁₀H₁₃IN₂O₂
• Molecular Weight: 320.13
• Mol file: 857266-59-2.mol

Synonyms:t-Butyl (5-iodopyridin-3-yl)carbamate;Tert-butyl (5-iodopyridin-3-yl)carbaMate

Chemical Property of t-Butyl (5-iodopyridin-3-yl)carbamate

Chemical Property:

• Vapor Pressure: 0.000307mmHg at 25°C
• Boiling Point: 321°C at 760 mmHg
• Flash Point: 147.9°C
• PSA: 51.22000
• Density: 1.652g/cm³
• LogP: 3.10620
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

98%min ^*data from raw suppliers

tert-Butyl(5-iodopyridin-3-yl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of t-Butyl (5-iodopyridin-3-yl)carbamate

There total 1 articles about t-Butyl (5-iodopyridin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(5-bromo-pyridin-3-yl)-carbamic acid tert-butyl ester (361550-43-8) → tert-butyl (5-iodopyridin-3-yl)carbamate (857266-59-2)

Guidance literature:

With N,N-dimethylethylenediamine; sodium iodide; copper(l) iodide; In 1,4-dioxane; at 110 ℃; for 24h;

upstream raw materials:

(5-bromo-pyridin-3-yl)-carbamic acid tert-butyl ester

Refernces

• 1、 -. "PYRIMIDINE COMPOUNDS HAVING TIES (TEK) INHIBITORY ACTIVITY". Page/Page column 107. . Retrieved 2008/06/13.