trans-4-(Boc-aMino)-3-Methoxypiperidine

Base Information

• Chemical Name: trans-4-(Boc-aMino)-3-Methoxypiperidine
• CAS No.: 1033748-33-2
• Molecular Formula: C11H22N2O3
• Molecular Weight: 230.30398
• Hs Code.: 2933399990
• Mol file: 1033748-33-2.mol

Synonyms:trans-4-(Boc-aMino)-3-Methoxypiperidine;tert-Butyl (trans-3-methoxypiperidin-4-yl)carbamate

Chemical Property of trans-4-(Boc-aMino)-3-Methoxypiperidine

Chemical Property:

• PSA: 63.08000
• LogP: 1.42120
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

trans-4-(Boc-amino)-3-methoxypiperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-4-(Boc-aMino)-3-Methoxypiperidine

There total 31 articles about trans-4-(Boc-aMino)-3-Methoxypiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl N-[(3R,4R)-1-benzyl-3-methoxy-4-piperidyl]carbamate → tert-butyl N-[(3R,4R)-3-methoxy-4-piperidyl]carbamate (907544-18-7,1033748-33-2)

Guidance literature:

With palladium 10% on activated carbon; ammonium formate; In methanol; at 50 ℃; for 1h;

DOI:10.1021/jm500462x

Reference yield: 100.0%

tert-butyl N-[(3S,4S)-1-benzyl-3-methoxy-4-piperidyl]carbamate → tert-butyl N-[(3S,4S)-3-methoxy-4-piperidyl]carbamate (1033748-33-2)

Guidance literature:

With palladium 10% on activated carbon; ammonium formate; In methanol; at 50 ℃; for 1h;

DOI:10.1021/jm500462x

Reference yield: 98.0%

benzyl trans(+/-)-4-[(tert-butoxycarbonyl)amino]-3-methoxypiperidine-1-carboxylate → tert-butyl [trans(+/-)-3-methoxypiperidin-4-yl]carbamate (1033748-33-2)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 1h;

upstream raw materials:

C₁₈H₂₈N₂O₃

di-tert-butyl dicarbonate

benzyl (3R,4R)-4-tert-butoxycarbonylamino-3-methoxy-piperidine-1-carboxylate

(3R,7aS)-3-phenyl-3,7a-dihydro-1H-pyrrolo[1,2-c]oxazol-5-one

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