4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI)

Base Information

Chemical Name:4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI)
CAS No.:324541-81-3
Molecular Formula:C₁₀H₁₆O₄
Molecular Weight:200.235
Hs Code.:
Mol file:324541-81-3.mol

Synonyms:4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI)

Chemical Property:

Melting Point:94 - 95 °C
PSA：47.92000
LogP:0.49120

Purity/Quality:

Safty Information:

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Technology Process of 4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI)

There total 37 articles about 4,8-Methano-1,3-dioxolo[4,5-d]oxepin-5-ol,hexahydro-2,2-dimethyl-,(3aS,4R,8R,8aR)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 112021-06-4
2α,3α-dihydroxy-di-O-isopropylidene-1β-hydroxymethyl-4β-(2-phenylstyryl)cyclopentane

: 324541-81-3,158413-30-0,158413-31-1
(1R,2R/S,5R,6R,7S)-6,7-Isopropylidenedioxy-3-oxabicyclo[3.2.1]octan-2-ol

Guidance literature:: With methylthiol; ozone; In dichloromethane; at -78 ℃; for 0.05h;

Reference yield: 88.0%

: 324541-79-9
(1R,2S,5S,6R,7S)-exo-6,7-Isopropylidenedioxybicyclo[3.2.1]oct-3-en-2-ol

: 324541-81-3,158413-30-0,158413-31-1
(1R,2R/S,5R,6R,7S)-6,7-Isopropylidenedioxy-3-oxabicyclo[3.2.1]octan-2-ol

Guidance literature:: (1R,2S,5S,6R,7S)-exo-6,7-Isopropylidenedioxybicyclo[3.2.1]oct-3-en-2-ol; With ozone; In methanol; at -78 ℃; for 0.333333h;

With sodium tetrahydroborate; In methanol; at -78 ℃; for 0.5h;

With sodium periodate; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2000-8717

Reference yield: 82.0%

: 324541-74-4
(-)-endo-6,7-Isopropylidenedioxybicyclo[3.2.1]oct-3-en-2-ol

: 324541-81-3,158413-30-0,158413-31-1
(1R,2R/S,5R,6R,7S)-6,7-Isopropylidenedioxy-3-oxabicyclo[3.2.1]octan-2-ol

Guidance literature:: (-)-endo-6,7-Isopropylidenedioxybicyclo[3.2.1]oct-3-en-2-ol; With ozone; In methanol; at -78 ℃; for 0.333333h;

With sodium tetrahydroborate; In methanol; at -78 ℃; for 0.5h;

With sodium periodate; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2000-8717