1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-

Base Information

• Chemical Name: 1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-
• CAS No.: 942920-60-7
• Molecular Formula: C₂₀H₂₁BN₂O₅S
• Molecular Weight: 412.274
• Mol file: 942920-60-7.mol

Synonyms:1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-

Chemical Property of 1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-

Chemical Property:

• PSA: 95.87000
• LogP: 3.46580

Purity/Quality:

97% ^*data from raw suppliers

1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-

There total 1 articles about 1H-PYRROLO[2,3-B]PYRIDINE-2-CARBOXALDEHYDE, 1-(PHENYLSULFONYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

→ 1-(phenylsulfonyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]-pyridine-2-carbaldehyde (942920-60-7)

Guidance literature:

Reference yield:

1-(phenylsulfonyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]-pyridine-2-carbaldehyde (942920-60-7) + N-[4-(4-bromo-1-ethyl-1H-pyrazol-3-yl)phenyl]-N0-phenylurea (942920-62-9) → N-(4-{4-[2-formyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-1-ethyl-1H-pyrazol-3-yl}phenyl)-N'-phenylurea (942920-61-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 100 ℃; for 17h;

DOI:10.1021/jm901870q

Downstream raw materials:

N-(4-{4-[2-formyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-1-ethyl-1H-pyrazol-3-yl}phenyl)-N'-phenylurea

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