6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI)

Base Information

Chemical Name:6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI)
CAS No.:468096-97-1
Molecular Formula:C₇H₁₁NO₃
Molecular Weight:157.169
Hs Code.:
Mol file:468096-97-1.mol

Synonyms:6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI)

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Chemical Property of 6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI)

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Technology Process of 6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI)

There total 5 articles about 6-Oxa-1-azabicyclo[3.1.0]hexane-2-carboxylicacid,ethylester,(2S,5R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172879-74-2
ethyl (S)-3,4-dihydro-2H-pyrrole-2-carboxylate

: 468096-98-2
ethyl (3S,5aS)-tetrahydropyrrolo[1,2-b]oxaziridine-3-carboxylate

: 468096-97-1
ethyl (3S,5aR)-tetrahydropyrrolo[1,2-b]oxaziridine-3-carboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform-d1; at 0 ℃; for 0.5h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(02)00110-6

Reference yield:

: 172879-73-1
ethyl (S)-3,4-dihydro-5-methylthio-2H-pyrrole-2-carboxylate

: 468096-97-1
ethyl (3S,5aR)-tetrahydropyrrolo[1,2-b]oxaziridine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / W-2 Raney-Ni / acetone / 1 h / Heating

2: m-chloroperbenzoic acid / CDCl₃ / 0.5 h / 0 °C

With W-2 Raney-Ni; 3-chloro-benzenecarboperoxoic acid; In chloroform-d1; acetone;
DOI:10.1016/S0957-4166(02)00110-6

Reference yield:

: 80442-95-1
ethyl (2S)-5-thioxo-3,4-dihydro-5H-pyrrole-2-carboxylate

: 468096-97-1
ethyl (3S,5aR)-tetrahydropyrrolo[1,2-b]oxaziridine-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / acetone / 18 h / 20 °C

2: 97 percent / aq. NaHCO₃ / CH₂Cl₂

3: 40 percent / W-2 Raney-Ni / acetone / 1 h / Heating

4: m-chloroperbenzoic acid / CDCl₃ / 0.5 h / 0 °C

With W-2 Raney-Ni; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform-d1; dichloromethane; acetone;
DOI:10.1016/S0957-4166(02)00110-6