N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE

Base Information

• Chemical Name: N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE
• CAS No.: 1414958-08-9
• Molecular Formula: C₁₀H₂₂N₂*ClH
• Molecular Weight: 206.759
• Mol file: 1414958-08-9.mol

Synonyms:N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE

Chemical Property of N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

Useful:

Technology Process of N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE

There total 2 articles about N,N-DIETHYL-CYCLOHEXANE-1,4-DIAMINE DIHYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl ((1r,4r)-4-(diethylamino)cyclohexyl)carbamate → (1r,4r)-N1,N1-diethylcyclohexane-1,4-diamine hydrochloride (1414958-08-9)

Guidance literature:

With hydrogenchloride; In water; ethyl acetate; at 25 ℃; for 0.166667h;

Reference yield:

trans-N-Boc-1,4-cyclohexanediamine (177906-48-8) → (1r,4r)-N1,N1-diethylcyclohexane-1,4-diamine hydrochloride (1414958-08-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / 1,2-dichloro-ethane / 1 h / 0 °C

1.2: 1 h / 0 - 25 °C

2.1: hydrogenchloride / water; ethyl acetate / 0.17 h / 25 °C

With hydrogenchloride; acetic acid; In water; ethyl acetate; 1,2-dichloro-ethane;

upstream raw materials:

trans-N-Boc-1,4-cyclohexanediamine

Refernces