5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST

Base Information

Chemical Name:5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST
CAS No.:17225-41-1
Molecular Formula:C32H44O5
Molecular Weight:508.698
Hs Code.:
Mol file:17225-41-1.mol

Synonyms:5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST;5B-cholanic acid-3A-ol-12-one*3-benzoate methyl E;5B-CHOLANIC ACID-3A-OL-12-ONE 3-BENZOATE METHYL ESTER);5beta-cholanic acid-3alpha-ol-12-one 3-benzoate methyl est

Suppliers and Price of 5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST

Chemical Property:

Melting Point:126-127 °C
Boiling Point:587.6±35.0 °C(Predicted)
PSA：69.67000
Density:1.14±0.1 g/cm3(Predicted)
LogP:6.63920

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST

There total 21 articles about 5B-CHOLANIC ACID-3A-OL-12-ONE3-BENZOATE METHYL EST which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 5969-28-8
3α-benzoyloxy-12α-hydroxy-5β-cholane-24-ic acid methyl ester

: 17225-41-1
3α-benzoyloxy-5β-cholane-12-one-24-ic acid methyl ester

Guidance literature:: With sodium dichromate; sulfuric acid; In diethyl ether; water; at 0 ℃; for 1.5h;
DOI:10.1016/S0040-4020(98)83048-2

Reference yield: 85.0%

: 3α-benzoyloxy-5β-chol-9(11)-ene-12-one-24-ic acid methyl ester

: 17225-41-1
3α-benzoyloxy-5β-cholane-12-one-24-ic acid methyl ester

Guidance literature:: 3α-benzoyloxy-5β-chol-9(11)-ene-12-one-24-ic acid methyl ester; With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 55 - 65 ℃; for 24h; under 9000.9 Torr; Autoclave;

With pyridinium chlorochromate; In tetrahydrofuran; ethyl acetate; at 20 - 30 ℃; for 12h;

With palladium on activated charcoal; hydrogen; at 55 - 65 ℃; for 24h; under 11251.1 Torr; Autoclave;

Reference yield:

: 3α-benzoyloxy-5β-chol-9(11)-ene-12-one-24-ic acid methyl ester

: 17225-41-1
3α-benzoyloxy-5β-cholane-12-one-24-ic acid methyl ester

: 98621-29-5,98621-30-8
3α-benzoxy-5β-cholo-9(11)-en-12-hydroxy-24-acid methyl ester

: 3α-benzoxy-5β-cholane-12β-hydroxy-24-acid methyl ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 55 - 65 ℃; for 24h; under 9000.9 Torr; Autoclave;