DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE

Base Information

• Chemical Name: DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE
• CAS No.: 82278-99-7
• Molecular Formula: C₁₅H₂₁NO₅
• Molecular Weight: 295.335
• Mol file: 82278-99-7.mol

Synonyms:DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE;Boc-3-Methoxy-DL-phenylalanine;2-([(TERT-BUTOXY)CARBONYL]AMINO)-3-(3-METHOXYPHENYL)PROPANOIC ACID

Chemical Property of DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE

Chemical Property:

• Boiling Point: 461.7±40.0 °C(Predicted)
• PKA: 3.89±0.10(Predicted)
• PSA: 84.86000
• Density: 1.168±0.06 g/cm3(Predicted)
• LogP: 2.60650

Purity/Quality:

99% ^*data from raw suppliers

2-((tert-Butoxycarbonyl)amino)-3-(3-methoxyphenyl)propanoicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE

There total 3 articles about DL-N-(TERT-BUTOXYCARBONYL)-3-METHOXYPHENYLALANINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

→ N-tert-butoxycarbonyl-3-methoxy-L-phenylalanine (261360-71-8,82278-99-7)

Guidance literature:

With potassium carbonate; In acetone; for 18h; Reflux;

With methanol; sodium hydroxide; at 40 ℃; for 3h;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (S)-2-amino-3-(3-methoxyphenyl)propanoic acid → N-tert-butoxycarbonyl-3-methoxy-L-phenylalanine (261360-71-8,82278-99-7)

Guidance literature:

With triethylamine; In tetrahydrofuran; water;

DOI:10.1016/j.bmc.2003.10.037

Reference yield:

→ (R)-2-((tert-butoxycarbonyl)amino)-3-(3-methoxyphenyl)propanoic acid (261380-37-4,82278-99-7)

Guidance literature:

upstream raw materials:

di-tert-butyl dicarbonate

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