1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE

Base Information

• Chemical Name: 1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE
• CAS No.: 401801-44-3
• Molecular Formula: C14H22N2O
• Molecular Weight: 234.34
• Hs Code.: 2933599090
• Mol file: 401801-44-3.mol

Synonyms:TIMTEC-BB SBB011706;ASINEX-REAG BAS 07435016;ASISCHEM C56781;1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE;AKOS BC-2669

Chemical Property of 1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE

Chemical Property:

• Boiling Point: 369.9±42.0 °C(Predicted)
• PKA: 9.13±0.10(Predicted)
• PSA: 24.50000
• Density: 1.009±0.06 g/cm3(Predicted)
• LogP: 1.85410

Purity/Quality:

98%min ^*data from raw suppliers

1-[2-(3,4-Dimethyl-phenoxy)-ethyl]-piperazine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE

There total 2 articles about 1-[2-(3,4-DIMETHYL-PHENOXY)-ETHYL]-PIPERAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

piperazine (110-85-0) + 1-bromo-2-(3,4-dimethylphenoxy)ethane (3351-53-9) → C14H22N2O (401801-44-3)

Guidance literature:

With hydrogen bromide; In ethanol; water; at 20 ℃; for 48h; Reflux;

DOI:10.1016/j.ejmech.2014.03.075

Reference yield:

3,4-Dimethylphenol (95-65-8) → C14H22N2O (401801-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 24 h / 50 °C / Reflux

2: hydrogen bromide / water; ethanol / 48 h / 20 °C / Reflux

With hydrogen bromide; potassium carbonate; In ethanol; water; acetonitrile;

DOI:10.1016/j.ejmech.2014.03.075

Reference yield:

2-chloro-N-(1,3-thiazol-2-yl)acetamide (5448-49-7) + C14H22N2O (401801-44-3) → N-(thiazol-2-yl)-2-(4-(2-(3,4-dimethylphenoxy)ethyl)piperazin-1-yl)acetamide (1352874-94-2)

Guidance literature:

With triethylamine; In chloroform; at 20 ℃; for 8h; Cooling with ice;

DOI:10.1016/j.ejmech.2014.03.075

upstream raw materials:

3,4-Dimethylphenol

piperazine

1-bromo-2-(3,4-dimethylphenoxy)ethane

Downstream raw materials:

N-(thiazol-2-yl)-2-(4-(2-(3,4-dimethylphenoxy)ethyl)piperazin-1-yl)acetamide

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