4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine

Base Information

• Chemical Name: 4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine
• CAS No.: 1207877-81-3
• Molecular Formula: C₁₇H₂₁N₃O
• Molecular Weight: 283.373
• Mol file: 1207877-81-3.mol

Synonyms:4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine

Chemical Property of 4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine

Chemical Property:

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Technology Process of 4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine

There total 1 articles about 4-methyl-3-[5-(4-morpholinylmethyl)-2-pyridinyl]benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine (882670-69-1) + 4-((6-bromopyridin-3-yl)methyl)morpholine (364793-93-1) → 4-methyl-3-(5-(morpholinomethyl)pyridin-2-yl)aniline (1207877-81-3)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 100 ℃; Inert atmosphere;

Reference yield:

bis(trichloromethyl) carbonate (32315-10-9) + 4-methyl-3-(5-(morpholinomethyl)pyridin-2-yl)aniline (1207877-81-3) → C18H20ClN3O2 (1207877-84-6)

Guidance literature:

With triethylamine; In DCM; at 20 ℃; for 0.3h; Cooling with ice;

upstream raw materials:

4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

4-((6-bromopyridin-3-yl)methyl)morpholine

Downstream raw materials:

C₁₈H₂₀ClN₃O₂

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