Benzene-1,3,5-triyltriboronic acid

Base Information

Chemical Name:Benzene-1,3,5-triyltriboronic acid
CAS No.:89641-21-4
Molecular Formula:C₆H₉B₃O₆
Molecular Weight:209.567
Hs Code.:
European Community (EC) Number:865-208-3
Nikkaji Number:J1.171.854J

Synonyms:BENZENE-1,3,5-TRIYLTRIBORONIC ACID;89641-21-4;Boronic acid, 1,3,5-benzenetriyltris-;(3,5-diboronophenyl)boronic acid;YSZC207;SCHEMBL806837;AMY027;benzene-1,3,5-triboronic acid;MFCD20275289;AKOS030627453;AS-47075;BENZENE-1,3,5-TRIYLTRIBORONICACID;DB-369813;CS-0111293;F11883;3,5-BIS(DIHYDROXYBORANYL)PHENYLBORONIC ACID

Suppliers and Price of Benzene-1,3,5-triyltriboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 20 raw suppliers

Chemical Property of Benzene-1,3,5-triyltriboronic acid

Chemical Property:

Hydrogen Bond Donor Count:6
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:210.0678285
Heavy Atom Count:15
Complexity:156

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C1=CC(=CC(=C1)B(O)O)B(O)O)(O)O

Technology Process of Benzene-1,3,5-triyltriboronic acid

There total 4 articles about Benzene-1,3,5-triyltriboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5624-60-2
1,3,5-tris(trimethylsilyl)benzene

: 7732-18-5
water

: 10294-33-4
boron tribromide

: 89641-21-4
benzene-1,3,5-triyltriboronic acid

Guidance literature:: 1,3,5-tris(trimethylsilyl)benzene; boron tribromide; at 100 ℃; for 4h; Inert atmosphere;

water; In hexane; at 0 ℃;

Reference yield: 95.0%

: 365564-05-2
1,3,5-tris(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

: 89641-21-4
benzene-1,3,5-triyltriboronic acid

Guidance literature:: 1,3,5-tris(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene; With sodium periodate; In tetrahydrofuran; water; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1002/anie.201308924

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 89641-21-4
benzene-1,3,5-triyltriboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium acetate; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 120 °C / Inert atmosphere; Schlenk technique

2.1: sodium periodate / tetrahydrofuran; water / 20 °C / Inert atmosphere; Schlenk technique

2.2: Inert atmosphere; Schlenk technique

With bis-triphenylphosphine-palladium(II) chloride; sodium periodate; potassium acetate; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1039/c8cc04870c