3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one

Base Information

Chemical Name:3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one
CAS No.:68931-37-3
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:
Mol file:68931-37-3.mol

Synonyms:3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one

Suppliers and Price of 3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one

Chemical Property:

PSA：17.07000
LogP:3.68020

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one

There total 4 articles about 3-[(E)-1,3-Butadienyl]-2,4,4,5-tetramethyl-2-cyclohexen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68931-36-2
4-Oxo-β-irol

: 68931-37-3
2-Methyl-megastigma-5,7(E),9-trien-4-on

Guidance literature:: With toluene-4-sulfonic acid; In toluene;
DOI:10.1002/hlca.19780610706

Reference yield:

: 202481-73-0,54082-69-8
4-(2,5,6,6-tetramethyl-2-cyclohexen-1-yl)-3-buten-2-one

: 68931-37-3
2-Methyl-megastigma-5,7(E),9-trien-4-on

Guidance literature:: Multi-step reaction with 4 steps

1: (i) aq. AcOOH, NaOAc, CH₂Cl₂, (ii) NaOMe, MeOH

2: aq. Na₂Cr₂O₇, H₂SO₄ / diethyl ether

3: NaBH₄ / methanol

4: TsOH / toluene

With sodium tetrahydroborate; sodium dichromate; sulfuric acid; toluene-4-sulfonic acid; In methanol; diethyl ether; toluene;
DOI:10.1002/hlca.19780610706

Reference yield:

: 68931-35-1
(E)-4-oxo-β-irone

: 68931-37-3
2-Methyl-megastigma-5,7(E),9-trien-4-on

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: TsOH / toluene

With sodium tetrahydroborate; toluene-4-sulfonic acid; In methanol; toluene;
DOI:10.1002/hlca.19780610706