α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate

Base Information

Chemical Name:α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate
CAS No.:66465-83-6
Molecular Formula:C₁₅H₂₄O₃
Molecular Weight:252.354
Hs Code.:

Synonyms:Acetic acid 1-methyl-2-[2,8,8-trimethyl-6-oxabicyclo[3.2.1]oct-2-en-7-yl]ethyl ester;α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate

Suppliers and Price of α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate

Chemical Property:

PSA：35.53000
LogP:3.08790

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate

There total 3 articles about α,2,8,8-Tetramethyl-6-oxabicyclo[3.2.1]oct-2-ene-7-ethanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67504-50-1
(-)-(2S)-2-hydroxy-β-ionone

: 66465-83-6
(2S,6R,7S)-2,7-epoxy-dihydro-α-ionyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / 0.5percent NaOEt / ethanol / 1 h / Heating

2: 962 mg / LAH / diethyl ether / 1 h / Heating

3: 1.12 g / pyridine / Ambient temperature

With lithium aluminium tetrahydride; sodium ethanolate; In pyridine; diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)90549-6

Reference yield:

: 108342-24-1
(2S,6R,7S)-(+)-2,7-epoxy-dihydro-α-ionone

: 66465-83-6
(2S,6R,7S)-2,7-epoxy-dihydro-α-ionyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 962 mg / LAH / diethyl ether / 1 h / Heating

2: 1.12 g / pyridine / Ambient temperature

With lithium aluminium tetrahydride; In pyridine; diethyl ether;
DOI:10.1016/S0040-4020(01)90549-6