4-Piperidinobenzaldehyde thiosemicarbazone

Base Information

Chemical Name:4-Piperidinobenzaldehyde thiosemicarbazone
CAS No.:63916-23-4
Molecular Formula:C13H18 N4 S
Molecular Weight:262.3738
Hs Code.:

Synonyms:4-Piperidinobenzaldehyde thiosemicarbazone;63916-23-4;BENZALDEHYDE, 4-PIPERIDINO-, THIOSEMICARBAZONE;[(E)-(4-piperidin-1-ylphenyl)methylideneamino]thiourea;(2E)-2-[4-(piperidin-1-yl)benzylidene]hydrazinecarbothioamide;Hydrazinecarbothioamide, 2-[[4-(1-piperidinyl)phenyl]methylene]-;STK029065;AKOS005380837;LS-25149

Suppliers and Price of 4-Piperidinobenzaldehyde thiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-PIPERIDINOBENZALDEHYDE THIOSEMICARBAZONE 95.00%
5MG
$ 503.73

Total 3 raw suppliers

Chemical Property of 4-Piperidinobenzaldehyde thiosemicarbazone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:105 - 106 °C
Boiling Point:443.2°Cat760mmHg
Flash Point:221.8°C
PSA：85.74000
Density:1.24g/cm³
LogP:3.00020
XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:262.12521776
Heavy Atom Count:18
Complexity:291

Purity/Quality:

99% ^*data from raw suppliers

4-PIPERIDINOBENZALDEHYDE THIOSEMICARBAZONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(CC1)C2=CC=C(C=C2)C=NNC(=S)N
Isomeric SMILES:C1CCN(CC1)C2=CC=C(C=C2)/C=N/NC(=S)N

Technology Process of 4-Piperidinobenzaldehyde thiosemicarbazone

There total 3 articles about 4-Piperidinobenzaldehyde thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 10338-57-5
4-(piperidin-1-yl)benzaldehyde

: 79-19-6
thiosemicarbazide

: 63916-23-4
1-[4-(piperidin-1-yl)benzylidene]thiosemicarbazide

Guidance literature:: With acetic acid; In ethanol; for 6h;
DOI:10.1007/s11164-018-3261-z

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 63916-23-4
1-[4-(piperidin-1-yl)benzylidene]thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 8 h / Reflux

2: acetic acid / ethanol / 6 h

With potassium carbonate; acetic acid; In ethanol; acetone;
DOI:10.1007/s11164-018-3261-z

Reference yield:

: 110-89-4
piperidine

: 63916-23-4
1-[4-(piperidin-1-yl)benzylidene]thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 8 h / Reflux

2: acetic acid / ethanol / 6 h

With potassium carbonate; acetic acid; In ethanol; acetone;
DOI:10.1007/s11164-018-3261-z