7-phenylbenzo[k]tetraphene

Base Information

Chemical Name:7-phenylbenzo[k]tetraphene
CAS No.:3781-43-9
Molecular Formula:C₂₈H₁₈
Molecular Weight:0
Hs Code.:
Mol file:3781-43-9.mol

Synonyms:NSC68425

Suppliers and Price of 7-phenylbenzo[k]tetraphene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 7-phenylbenzo[k]tetraphene

Chemical Property:

Vapor Pressure:2.05E-12mmHg at 25°C
Boiling Point:570°C at 760 mmHg
Flash Point:295.8°C
Density:1.217g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7-phenylbenzo[k]tetraphene

There total 7 articles about 7-phenylbenzo[k]tetraphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 108-86-1,52753-63-6
bromobenzene

: 7-chlorobenzo[k]tetraphene

: 3781-43-9
7-phenylbenzo[k]tetraphene

Guidance literature:: bromobenzene; With magnesium; In tetrahydrofuran; Inert atmosphere;

7-chlorobenzo[k]tetraphene; With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; In tetrahydrofuran; at 20 ℃; for 1h; regiospecific reaction; Inert atmosphere;
DOI:10.1002/chem.201501861

Reference yield:

: 3580-70-9
2-<1-Naphthylmethyl>-1-naphthophenon

: 3781-43-9
7-phenylbenzo[k]tetraphene

Guidance literature:: With hydrogen bromide; In acetic acid; at 180 ℃;
DOI:10.1021/jo01019a512

Reference yield:

: 90-11-9
1-Bromonaphthalene

: 3781-43-9
7-phenylbenzo[k]tetraphene

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Mg, (ii) /BRN= 1943405/

2: (i) Mg, (ii) /BRN= 471389/

3: aq. HBr / acetic acid / 180 °C

With hydrogen bromide; In acetic acid;
DOI:10.1021/jo01019a512